ethyl <6-amino-4-<<2-(4-methoxyphenyl)-1-methyl-2-oxoethyl>amino>-5-nitropyridin-2-yl>carbamate oxime

Base Information

Chemical Name:ethyl <6-amino-4-<<2-(4-methoxyphenyl)-1-methyl-2-oxoethyl>amino>-5-nitropyridin-2-yl>carbamate oxime
CAS No.:139016-58-3
Molecular Formula:C₁₈H₂₂N₆O₆
Molecular Weight:418.409
Hs Code.:

Synonyms:ethyl <6-amino-4-<<2-(4-methoxyphenyl)-1-methyl-2-oxoethyl>amino>-5-nitropyridin-2-yl>carbamate oxime

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Chemical Property of ethyl <6-amino-4-<<2-(4-methoxyphenyl)-1-methyl-2-oxoethyl>amino>-5-nitropyridin-2-yl>carbamate oxime

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Technology Process of ethyl <6-amino-4-<<2-(4-methoxyphenyl)-1-methyl-2-oxoethyl>amino>-5-nitropyridin-2-yl>carbamate oxime

There total 4 articles about ethyl <6-amino-4-<<2-(4-methoxyphenyl)-1-methyl-2-oxoethyl>amino>-5-nitropyridin-2-yl>carbamate oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 6506-86-1
ethyl (6-amino-4-chloro-5-nitropyridin-2-yl)carbamate

: 143858-98-4
2-amino-4'-methoxypropiophenone oxime

: 139016-58-3
ethyl <6-amino-4-<<2-(4-methoxyphenyl)-1-methyl-2-oxoethyl>amino>-5-nitropyridin-2-yl>carbamate oxime

Guidance literature:: With triethylamine; In ethanol; for 11.5h; Heating;
DOI:10.1021/jm00084a003

Reference yield:

: 21086-33-9
2-bromo-1-(4-methoxyphenyl)-1-propanone

: 139016-58-3
ethyl <6-amino-4-<<2-(4-methoxyphenyl)-1-methyl-2-oxoethyl>amino>-5-nitropyridin-2-yl>carbamate oxime

Guidance literature:: Multi-step reaction with 4 steps

1: N,N-dimethyl-acetamide / 8 h / Ambient temperature

2: hydroxylamine hydrochloride, pyridine / ethanol / 4 h / Heating

3: 1.) hydrazine, 2.) 1N aq. HCl / 1.) EtOH, 45 deg C, 21 h, 2.) EtOH, from 0 deg C to 5 deg C, 1 h

4: 80 percent / Et₃N / ethanol / 11.5 h / Heating

With pyridine; hydrogenchloride; hydroxylamine hydrochloride; triethylamine; hydrazine; In ethanol; N,N-dimethyl acetamide;
DOI:10.1021/jm00084a003

Reference yield:

: 19427-11-3
(4-Methoxyphenyl)-(1-phthalimidoethyl)-keton

: 139016-58-3
ethyl <6-amino-4-<<2-(4-methoxyphenyl)-1-methyl-2-oxoethyl>amino>-5-nitropyridin-2-yl>carbamate oxime

Guidance literature:: Multi-step reaction with 3 steps

1: hydroxylamine hydrochloride, pyridine / ethanol / 4 h / Heating

2: 1.) hydrazine, 2.) 1N aq. HCl / 1.) EtOH, 45 deg C, 21 h, 2.) EtOH, from 0 deg C to 5 deg C, 1 h

3: 80 percent / Et₃N / ethanol / 11.5 h / Heating

With pyridine; hydrogenchloride; hydroxylamine hydrochloride; triethylamine; hydrazine; In ethanol;
DOI:10.1021/jm00084a003