2,6-dimethyl-4-(3'-nitrophenyl)1,4-dihydropyridine-3,5-dicarboxylic acid 3-ethyl ester-5-allyl ester

Base Information

Chemical Name:2,6-dimethyl-4-(3'-nitrophenyl)1,4-dihydropyridine-3,5-dicarboxylic acid 3-ethyl ester-5-allyl ester
CAS No.:39562-23-7
Molecular Formula:C₂₀H₂₂N₂O₆
Molecular Weight:386.404
Hs Code.:

Synonyms:2,6-dimethyl-4-(3'-nitrophenyl)1,4-dihydropyridine-3,5-dicarboxylic acid 3-ethyl ester-5-allyl ester

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Chemical Property of 2,6-dimethyl-4-(3'-nitrophenyl)1,4-dihydropyridine-3,5-dicarboxylic acid 3-ethyl ester-5-allyl ester

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Technology Process of 2,6-dimethyl-4-(3'-nitrophenyl)1,4-dihydropyridine-3,5-dicarboxylic acid 3-ethyl ester-5-allyl ester

There total 6 articles about 2,6-dimethyl-4-(3'-nitrophenyl)1,4-dihydropyridine-3,5-dicarboxylic acid 3-ethyl ester-5-allyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 70076-42-5
3-nitrobenzylidene acetoacetic acid ethyl ester

: 1118-84-9
allyl acetoacetate

: 39562-23-7
2,6-dimethyl-4-(3'-nitrophenyl)1,4-dihydropyridine-3,5-dicarboxylic acid 3-ethyl ester-5-allyl ester

Guidance literature:: With ammonia; In ethanol;

Reference yield:

: 1118-84-9
allyl acetoacetate

: 39562-23-7
2,6-dimethyl-4-(3'-nitrophenyl)1,4-dihydropyridine-3,5-dicarboxylic acid 3-ethyl ester-5-allyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: gaseous NH₃, p-toluenesulfonic acid / toluene / Heating

2: ethanol / Heating

With ammonia; toluene-4-sulfonic acid; In ethanol; toluene;

Reference yield:

: 141-97-9
ethyl acetoacetate

: 39562-23-7
2,6-dimethyl-4-(3'-nitrophenyl)1,4-dihydropyridine-3,5-dicarboxylic acid 3-ethyl ester-5-allyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: gaseous HCl / toluene / 40 h / Ambient temperature

2: ethanol / Heating

With hydrogenchloride; In ethanol; toluene;