5-(tert-butoxy)-2-(4-(2,7-difluoro-6-hydroxy-3-oxo-3H-xanthen-9-yl)-3-methylbenzamido)-5-oxopentanoic acid

Base Information

Chemical Name:5-(tert-butoxy)-2-(4-(2,7-difluoro-6-hydroxy-3-oxo-3H-xanthen-9-yl)-3-methylbenzamido)-5-oxopentanoic acid
CAS No.:1264272-63-0
Molecular Formula:C₃₀H₂₇F₂NO₈
Molecular Weight:567.543
Hs Code.:

Synonyms:5-(tert-butoxy)-2-(4-(2,7-difluoro-6-hydroxy-3-oxo-3H-xanthen-9-yl)-3-methylbenzamido)-5-oxopentanoic acid

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Chemical Property of 5-(tert-butoxy)-2-(4-(2,7-difluoro-6-hydroxy-3-oxo-3H-xanthen-9-yl)-3-methylbenzamido)-5-oxopentanoic acid

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Technology Process of 5-(tert-butoxy)-2-(4-(2,7-difluoro-6-hydroxy-3-oxo-3H-xanthen-9-yl)-3-methylbenzamido)-5-oxopentanoic acid

There total 2 articles about 5-(tert-butoxy)-2-(4-(2,7-difluoro-6-hydroxy-3-oxo-3H-xanthen-9-yl)-3-methylbenzamido)-5-oxopentanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 952053-74-6
1-{[4-(2,7-difluoro-6-hydroxy-3-oxo-xanthen-9-yl)-3-methylbenzoyl]oxy}pyrrolidine-2,5-dione

: 2419-56-9
L-glutamic acid 5-tert-butyl ester

: 1264272-63-0
5-(tert-butoxy)-2-(4-(2,7-difluoro-6-hydroxy-3-oxo-3H-xanthen-9-yl)-3-methylbenzamido)-5-oxopentanoic acid

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 22 ℃; for 16h;

Reference yield:

: 71989-18-9
Fmoc-Glu(OtBu)-OH

: 1264272-63-0
5-(tert-butoxy)-2-(4-(2,7-difluoro-6-hydroxy-3-oxo-3H-xanthen-9-yl)-3-methylbenzamido)-5-oxopentanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: piperidine / N,N-dimethyl-formamide / 0.5 h

2: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 16 h / 22 °C

With piperidine; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide;