5-<(3-carboxyphenyl)(hydroxyimino)methyl>-2-<(6-phenylhexyl)oxy>benzenepropanoic acid

Base Information

Chemical Name:5-<(3-carboxyphenyl)(hydroxyimino)methyl>-2-<(6-phenylhexyl)oxy>benzenepropanoic acid
CAS No.:128950-01-6
Molecular Formula:C₂₉H₃₁NO₆
Molecular Weight:489.568
Hs Code.:

Synonyms:5-<(3-carboxyphenyl)(hydroxyimino)methyl>-2-<(6-phenylhexyl)oxy>benzenepropanoic acid

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Chemical Property of 5-<(3-carboxyphenyl)(hydroxyimino)methyl>-2-<(6-phenylhexyl)oxy>benzenepropanoic acid

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Technology Process of 5-<(3-carboxyphenyl)(hydroxyimino)methyl>-2-<(6-phenylhexyl)oxy>benzenepropanoic acid

There total 5 articles about 5-<(3-carboxyphenyl)(hydroxyimino)methyl>-2-<(6-phenylhexyl)oxy>benzenepropanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 117424-97-2
5-(3-carboxybenzoyl)-2-<(6-phenylhexyl)oxy>benzenepropanoic acid

: 128950-01-6
5-<(3-carboxyphenyl)(hydroxyimino)methyl>-2-<(6-phenylhexyl)oxy>benzenepropanoic acid

Guidance literature:: With pyridine; hydroxylamine hydrochloride; at 70 ℃; for 1h;
DOI:10.1021/jm00172a019

Reference yield:

: 67326-20-9
3-carbethoxybenzoyl chloride

: 128950-01-6
5-<(3-carboxyphenyl)(hydroxyimino)methyl>-2-<(6-phenylhexyl)oxy>benzenepropanoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 56 percent / AlCl₃ / CH₂Cl₂ / 1 h / 0 - 25 °C

2: 92 percent / pyridine hydrochloride / 4 h / 180 °C

3: 1.) NaH / 1.) DMF, 25 deg C, 30 min, 2.) 65 deg C, overnight

4: 74 percent / hydroxylamine hydrochloride, pyridine / 1 h / 70 °C

With pyridine; aluminium trichloride; hydroxylamine hydrochloride; pyridine hydrochloride; sodium hydride; In dichloromethane;
DOI:10.1021/jm00172a019

Reference yield:

: 70311-27-2
2-methoxybenzenepropanoic acid ethyl ester

: 128950-01-6
5-<(3-carboxyphenyl)(hydroxyimino)methyl>-2-<(6-phenylhexyl)oxy>benzenepropanoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 56 percent / AlCl₃ / CH₂Cl₂ / 1 h / 0 - 25 °C

2: 92 percent / pyridine hydrochloride / 4 h / 180 °C

3: 1.) NaH / 1.) DMF, 25 deg C, 30 min, 2.) 65 deg C, overnight

4: 74 percent / hydroxylamine hydrochloride, pyridine / 1 h / 70 °C

With pyridine; aluminium trichloride; hydroxylamine hydrochloride; pyridine hydrochloride; sodium hydride; In dichloromethane;
DOI:10.1021/jm00172a019