[(S)-2-(Acetyl-methyl-amino)-1-hydroxymethyl-ethyl]-carbamic acid benzyl ester

Base Information

Chemical Name:[(S)-2-(Acetyl-methyl-amino)-1-hydroxymethyl-ethyl]-carbamic acid benzyl ester
CAS No.:211756-47-7
Molecular Formula:C₁₄H₂₀N₂O₄
Molecular Weight:280.324
Hs Code.:

Synonyms:[(S)-2-(Acetyl-methyl-amino)-1-hydroxymethyl-ethyl]-carbamic acid benzyl ester

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Chemical Property of [(S)-2-(Acetyl-methyl-amino)-1-hydroxymethyl-ethyl]-carbamic acid benzyl ester

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Technology Process of [(S)-2-(Acetyl-methyl-amino)-1-hydroxymethyl-ethyl]-carbamic acid benzyl ester

There total 5 articles about [(S)-2-(Acetyl-methyl-amino)-1-hydroxymethyl-ethyl]-carbamic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 211756-46-6
(S)-3-(Acetyl-methyl-amino)-2-benzyloxycarbonylamino-propionic acid methyl ester

: 211756-47-7
[(S)-2-(Acetyl-methyl-amino)-1-hydroxymethyl-ethyl]-carbamic acid benzyl ester

Guidance literature:: With sodium tetrahydroborate; lithium chloride; In tetrahydrofuran; ethanol; Ambient temperature;
DOI:10.1021/jm980071x

Reference yield:

: 35761-26-3
(S)-3-amino-2-(((benzyloxy)carbonyl)amino)propanoic acid

: 211756-47-7
[(S)-2-(Acetyl-methyl-amino)-1-hydroxymethyl-ethyl]-carbamic acid benzyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 99 percent / HCl gas / 12 h / Ambient temperature

2: 74 percent / H₂O / 12 h / Ambient temperature

3: 95 percent / Et₃SiH, TFA / CH₂Cl₂ / 2 h / Ambient temperature

4: 89 percent / pyridine / 12 h / Ambient temperature

5: LiCl, NaBH₄ / tetrahydrofuran; ethanol / Ambient temperature

With pyridine; hydrogenchloride; triethylsilane; sodium tetrahydroborate; trifluoroacetic acid; lithium chloride; In tetrahydrofuran; ethanol; dichloromethane; water;
DOI:10.1021/jm980071x

Reference yield:

: 35761-27-4,96192-93-7
methyl (2S)-3-amino-2-{[(benzyloxy)carbonyl]amino}propanoate hydrochloride

: 211756-47-7
[(S)-2-(Acetyl-methyl-amino)-1-hydroxymethyl-ethyl]-carbamic acid benzyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 74 percent / H₂O / 12 h / Ambient temperature

2: 95 percent / Et₃SiH, TFA / CH₂Cl₂ / 2 h / Ambient temperature

3: 89 percent / pyridine / 12 h / Ambient temperature

4: LiCl, NaBH₄ / tetrahydrofuran; ethanol / Ambient temperature

With pyridine; triethylsilane; sodium tetrahydroborate; trifluoroacetic acid; lithium chloride; In tetrahydrofuran; ethanol; dichloromethane; water;
DOI:10.1021/jm980071x