Technology Process of C13H18N2O
There total 6 articles about C13H18N2O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C13H16N2;
With
water; potassium hydroxide;
In
ethanol;
at 150 ℃;
for 0.166667h;
Microwave irradiation;
With
hydrogenchloride;
In
ethanol; water;
pH=7;
DOI:10.1055/s-0033-1340250
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium tetrahydroborate / methanol / 20 °C
2.1: acetonitrile / 15 h / Reflux
3.1: acetonitrile / 24 h / Reflux
4.1: potassium hydroxide; water / ethanol / 0.17 h / 150 °C / Microwave irradiation
4.2: pH 7
With
sodium tetrahydroborate; water; potassium hydroxide;
In
methanol; ethanol; acetonitrile;
DOI:10.1055/s-0033-1340250
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: bromine / dichloromethane / 2.5 h / 0 - 20 °C
2.1: titanium tetrachloride; triethylamine / diethyl ether / 15 h / 0 - 20 °C
3.1: sodium tetrahydroborate / methanol / 20 °C
4.1: acetonitrile / 15 h / Reflux
5.1: acetonitrile / 24 h / Reflux
6.1: potassium hydroxide; water / ethanol / 0.17 h / 150 °C / Microwave irradiation
6.2: pH 7
With
sodium tetrahydroborate; water; bromine; titanium tetrachloride; triethylamine; potassium hydroxide;
In
methanol; diethyl ether; ethanol; dichloromethane; acetonitrile;
DOI:10.1055/s-0033-1340250
