1,1-Dichloro-2-propene

Base Information

Chemical Name:1,1-Dichloro-2-propene
CAS No.:167558-63-6
Molecular Formula:C₁₁H₁₂Cl₂OS
Molecular Weight:263.188
Hs Code.:

1,1-Dichloro-2-<o-(methoxymethylthio)phenyl>propene

Synonyms:1,1-Dichloro-2-propene

Suppliers and Price of 1,1-Dichloro-2-propene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,1-Dichloro-2-propene

Chemical Property:

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Technology Process of 1,1-Dichloro-2-propene

There total 3 articles about 1,1-Dichloro-2-propene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 866-23-9
diethyl (trichloromethyl)phosphonate

: 167558-61-4
o-(Methoxymethylthio)acetophenone

: 167558-63-6
1,1-Dichloro-2-propene

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; 1.) -90 deg C, 15 min, 2.) r.t., overnight;
DOI:10.1021/jo00122a046

Reference yield:

: 26824-02-2
1-(2-mercaptophenyl)ethan-1-one

: 167558-63-6
1,1-Dichloro-2-propene

Guidance literature:: Multi-step reaction with 2 steps

1: KOt-Bu / tetrahydrofuran / 1.) 15 min, 2.) 2 h

2: 65 percent / n-BuLi / tetrahydrofuran; hexane / 1.) -90 deg C, 15 min, 2.) r.t., overnight

With n-butyllithium; potassium tert-butylate; In tetrahydrofuran; hexane;
DOI:10.1021/jo00122a046

Reference yield:

: 147-93-3
Thiosalicylic acid

: 167558-63-6
1,1-Dichloro-2-propene

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / MeLi / diethyl ether; tetrahydrofuran / Ambient temperature

2: KOt-Bu / tetrahydrofuran / 1.) 15 min, 2.) 2 h

3: 65 percent / n-BuLi / tetrahydrofuran; hexane / 1.) -90 deg C, 15 min, 2.) r.t., overnight

With n-butyllithium; potassium tert-butylate; methyllithium; In tetrahydrofuran; diethyl ether; hexane;
DOI:10.1021/jo00122a046