2-trifluoroacetamidoethyl 2,2',3,6,6'-penta-O-benzyl-3',4'-O-isopropylidene-β-D-lactoside

Base Information

Chemical Name:2-trifluoroacetamidoethyl 2,2',3,6,6'-penta-O-benzyl-3',4'-O-isopropylidene-β-D-lactoside
CAS No.:309935-03-3
Molecular Formula:C₅₄H₆₀F₃NO₁₂
Molecular Weight:972.065
Hs Code.:

Synonyms:2-trifluoroacetamidoethyl 2,2',3,6,6'-penta-O-benzyl-3',4'-O-isopropylidene-β-D-lactoside

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Chemical Property of 2-trifluoroacetamidoethyl 2,2',3,6,6'-penta-O-benzyl-3',4'-O-isopropylidene-β-D-lactoside

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Technology Process of 2-trifluoroacetamidoethyl 2,2',3,6,6'-penta-O-benzyl-3',4'-O-isopropylidene-β-D-lactoside

There total 2 articles about 2-trifluoroacetamidoethyl 2,2',3,6,6'-penta-O-benzyl-3',4'-O-isopropylidene-β-D-lactoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 383-63-1
ethyl trifluoroacetate,

: 2-[(2R,3R,4S,5R,6R)-3,4-Bis-benzyloxy-5-((3aS,4R,6S,7R,7aS)-7-benzyloxy-4-benzyloxymethyl-2,2-dimethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-6-yloxy)-6-benzyloxymethyl-tetrahydro-pyran-2-yloxy]-ethylamine

: 309935-03-3
2-trifluoroacetamidoethyl 2,2',3,6,6'-penta-O-benzyl-3',4'-O-isopropylidene-β-D-lactoside

Guidance literature:: With triethylamine; In methanol; at 20 ℃; for 15h;
DOI:10.1007/BF02495780

Reference yield:

: 2-oximinoethyl 2,2',3,6,6'-penta-O-benzyl-3',4'-O-isopropylidene-β-D-lactoside

: 309935-03-3
2-trifluoroacetamidoethyl 2,2',3,6,6'-penta-O-benzyl-3',4'-O-isopropylidene-β-D-lactoside

Guidance literature:: Multi-step reaction with 2 steps

1: LiAlH₄ / tetrahydrofuran

2: 92 percent / Et₃N / methanol / 15 h / 20 °C

With lithium aluminium tetrahydride; triethylamine; In tetrahydrofuran; methanol; 1: Reduction / 2: Acylation;
DOI:10.1007/BF02495780