Technology Process of C31H54O3Si2
There total 1 articles about C31H54O3Si2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
tert-butyl[(1S)-3-iodo-1-phenethylpropyl]oxydimethylsilane;
With
tert.-butyl lithium;
In
diethyl ether; hexane;
at -78 ℃;
for 4h;
Inert atmosphere;
(R)-2-allyl-4-(tert-butyldimethylsilyloxy)cyclopent-2-enone;
With
methyllithium; copper(l) cyanide;
In
diethyl ether; hexane;
at -78 - -50 ℃;
for 0.916667h;
Inert atmosphere;
- Guidance literature:
-
C31H54O3Si2;
With
diisobutylaluminium hydride;
In
toluene;
at -78 ℃;
for 3h;
With
methanol; sulfuric acid; water;
In
toluene;
at -50 ℃;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: diisobutylaluminium hydride / toluene / 3 h / -78 °C
1.2: -50 °C
2.1: dmap; diisopropyl-carbodiimide / tetrahydrofuran / 24 h / 20 - 40 °C
3.1: Grubbs catalyst first generation / dichloromethane / 18 h / 20 - 40 °C / Inert atmosphere
4.1: tetrabutyl ammonium fluoride; ammonium hydrogen difluoride / tetrahydrofuran / 24 h / 20 - 40 °C
5.1: sodium hydride / isopropyl alcohol; mineral oil / 18 h / 20 - 35 °C
5.2: 18 h / 20 °C
With
dmap; ammonium hydrogen difluoride; tetrabutyl ammonium fluoride; sodium hydride; diisobutylaluminium hydride; diisopropyl-carbodiimide;
Grubbs catalyst first generation;
In
tetrahydrofuran; dichloromethane; isopropyl alcohol; toluene; mineral oil;
![tert-butyl[(1S)-3-iodo-1-phenethylpropyl]oxydimethylsilane](/Databaselist/images/loading.webp)
