4-((benzenesulfonyl)methyl)-2-methoxy-3,3a,4,6a-tetrahydro-2H-cyclopenta[b]furan

Base Information

Chemical Name:4-((benzenesulfonyl)methyl)-2-methoxy-3,3a,4,6a-tetrahydro-2H-cyclopenta[b]furan
CAS No.:807355-29-9
Molecular Formula:C₁₅H₁₈O₄S
Molecular Weight:294.372
Hs Code.:

Synonyms:4-((benzenesulfonyl)methyl)-2-methoxy-3,3a,4,6a-tetrahydro-2H-cyclopenta[b]furan

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-((benzenesulfonyl)methyl)-2-methoxy-3,3a,4,6a-tetrahydro-2H-cyclopenta[b]furan

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Technology Process of 4-((benzenesulfonyl)methyl)-2-methoxy-3,3a,4,6a-tetrahydro-2H-cyclopenta[b]furan

There total 5 articles about 4-((benzenesulfonyl)methyl)-2-methoxy-3,3a,4,6a-tetrahydro-2H-cyclopenta[b]furan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 807355-28-8
2-methoxy-4-((phenylsulfanyl)methyl)-3,3a,4,6a-tetrahydro-2H-cyclopenta[b]furan

: 807355-29-9
4-((benzenesulfonyl)methyl)-2-methoxy-3,3a,4,6a-tetrahydro-2H-cyclopenta[b]furan

Guidance literature:: With ammonium molibdate; dihydrogen peroxide; In methanol; water; at 20 ℃; for 17.5h;
DOI:10.1021/jo050423p

Reference yield:

: (-)-(3aS,4S,6aR)-4-hydroxymethyl-3,3a,4,6a-tetrahydro-cyclopenta[b]furan-2-one

: 807355-29-9
4-((benzenesulfonyl)methyl)-2-methoxy-3,3a,4,6a-tetrahydro-2H-cyclopenta[b]furan

Guidance literature:: Multi-step reaction with 4 steps

1: 92 percent / n-Bu₃P / tetrahydrofuran / 4 h / 20 °C

2: DIBAL-H / CH₂Cl₂; hexane / 1 h / -78 °C

3: 403 mg / PTSA / 18 h / -20 °C

4: 98 percent / (NH₄)2MoO₄; H₂O₂ / methanol; H₂O / 17.5 h / 20 °C

With ammonium molibdate; tributylphosphine; dihydrogen peroxide; diisobutylaluminium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; hexane; dichloromethane; water;
DOI:10.1021/jo050423p

Reference yield:

: 807355-27-7
4-((phenylsulfanyl)methyl)-3,3a,4,6a-tetrahydro-cyclopenta[b]furan-2-one

: 807355-29-9
4-((benzenesulfonyl)methyl)-2-methoxy-3,3a,4,6a-tetrahydro-2H-cyclopenta[b]furan

Guidance literature:: Multi-step reaction with 3 steps

1: DIBAL-H / CH₂Cl₂; hexane / 1 h / -78 °C

2: 403 mg / PTSA / 18 h / -20 °C

3: 98 percent / (NH₄)2MoO₄; H₂O₂ / methanol; H₂O / 17.5 h / 20 °C

With ammonium molibdate; dihydrogen peroxide; diisobutylaluminium hydride; toluene-4-sulfonic acid; In methanol; hexane; dichloromethane; water;
DOI:10.1021/jo050423p