(2S,1'R)-N-[1'-(2-Furyl)-3'-phenylpropyl]-N-(2-hydroxyethyl)-2-phenylglycinol

Base Information

• Chemical Name: (2S,1'R)-N-[1'-(2-Furyl)-3'-phenylpropyl]-N-(2-hydroxyethyl)-2-phenylglycinol
• CAS No.: 308245-73-0
• Molecular Formula: C₂₃H₂₇NO₃
• Molecular Weight: 365.472

Synonyms:(2S,1'R)-N-[1'-(2-Furyl)-3'-phenylpropyl]-N-(2-hydroxyethyl)-2-phenylglycinol

Chemical Property of (2S,1'R)-N-[1'-(2-Furyl)-3'-phenylpropyl]-N-(2-hydroxyethyl)-2-phenylglycinol

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Technology Process of (2S,1'R)-N-[1'-(2-Furyl)-3'-phenylpropyl]-N-(2-hydroxyethyl)-2-phenylglycinol

There total 3 articles about (2S,1'R)-N-[1'-(2-Furyl)-3'-phenylpropyl]-N-(2-hydroxyethyl)-2-phenylglycinol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

(5S,1'S)-N-[1'-(2-Furyl)-3'-phenylpropyl]-5-phenylmorpholin-2-one (182161-99-5) → (2S,1'R)-N-[1'-(2-Furyl)-3'-phenylpropyl]-N-(2-hydroxyethyl)-2-phenylglycinol (308245-73-0)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; for 1.5h; Heating;

DOI:10.1039/b003067h

Reference yield:

3-phenyl-propionaldehyde (104-53-0) → (2S,1'R)-N-[1'-(2-Furyl)-3'-phenylpropyl]-N-(2-hydroxyethyl)-2-phenylglycinol (308245-73-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 66 percent / tetrahydrofuran / 2 h / Heating

2: 99 percent / LiAlH₄ / diethyl ether / 1.5 h / Heating

With lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether; 1: Condensation / 2: Reduction;

DOI:10.1039/b003067h

Reference yield:

(5S)-5-phenylmorpholin-2-one (144896-92-4,134872-85-8) → (2S,1'R)-N-[1'-(2-Furyl)-3'-phenylpropyl]-N-(2-hydroxyethyl)-2-phenylglycinol (308245-73-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 66 percent / tetrahydrofuran / 2 h / Heating

2: 99 percent / LiAlH₄ / diethyl ether / 1.5 h / Heating

With lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether; 1: Condensation / 2: Reduction;

DOI:10.1039/b003067h

upstream raw materials:

(5S,1'S)-N-[1'-(2-Furyl)-3'-phenylpropyl]-5-phenylmorpholin-2-one

3-phenyl-propionaldehyde

(5S)-5-phenylmorpholin-2-one

Downstream raw materials:

(R)-N-[1'-(2-Furyl)-3'-phenyloropyl]-2-aminoethanol

(R)-N-[1'-(2-Furyl)-3'-phenylpropyl]-N-(2-phenylselenoethyl)toluene-p-sulfonamide

(R)-N-[1'-(2-Furyl)-3'-phenylpropyl]toluene-p-sulfonamide

(R)-4-Phenyl-2-(toluene-4-sulfonylamino)-butyric acid

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