C₅₃H₆₄N₂O₂₂S

Base Information

Chemical Name:C₅₃H₆₄N₂O₂₂S
CAS No.:872120-79-1
Molecular Formula:C₅₃H₆₄N₂O₂₂S
Molecular Weight:1113.16
Hs Code.:

C<sub>53</sub>H<sub>64</sub>N<sub>2</sub>O<sub>22</sub>S

Synonyms:C₅₃H₆₄N₂O₂₂S

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Chemical Property of C₅₃H₆₄N₂O₂₂S

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Technology Process of C₅₃H₆₄N₂O₂₂S

There total 12 articles about C₅₃H₆₄N₂O₂₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 872120-78-0
C₅₆H₆₅Cl₃N₂O₂₄S

: 872120-79-1
C₅₃H₆₄N₂O₂₂S

Guidance literature:: With zinc; In tetrahydrofuran; at 20 ℃; for 28h;
DOI:10.1002/anie.200501608

Reference yield:

: 872120-64-4
(1S,3R,4R,8S)-8-Hydroxy-3-[(S)-hydroxy-((R)-2-phenyl-[1,3]dioxolan-4-yl)-methyl]-1-phenylsulfanyl-2-oxa-5-aza-bicyclo[2.2.2]octan-6-one

: 872120-79-1
C₅₃H₆₄N₂O₂₂S

Guidance literature:: Multi-step reaction with 8 steps

1: pyridine; 4-dimethylaminopyridine / 3 h / 20 °C

2: 1.38 g / hydrazinium acetate / tetrahydrofuran / 1.33 h / 20 °C

3: 74 percent / BH₃*NMe₃; AlCl₃; molecular sieves 4 Angstroem / tetrahydrofuran / 6 h / 0 - 20 °C

4: 49 percent / N-iodosuccinimide; trifluoromethanesulfonic acid; molecular sieves 3 Angstroem / various solvent(s) / 5 h / -80 °C

5: 79 percent / pyridine; 4-dimethylaminopyridine / 42 h / 40 °C

6: trimethylamine / acetonitrile; H₂O / 48 h / 40 °C

7: 380 mg / potassium carbonate / dimethylformamide / 3 h / 20 °C

8: 94 percent / zinc / tetrahydrofuran / 28 h / 20 °C

With pyridine; dmap; N-iodo-succinimide; aluminium trichloride; trifluorormethanesulfonic acid; trimethylamine-borane; 3 A molecular sieve; 4 A molecular sieve; hydrazinium monoacetate; potassium carbonate; zinc; trimethylamine; In tetrahydrofuran; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/anie.200501608

Reference yield:

: 872120-66-6
phenyl 5-amino-4,7-di-O-acetyl-9-O-benzyl-3,5-dideoxy-2-thio-D-glycero-α-D-galacto-2-nonulopyranoside-1,5-lactam

: 872120-79-1
C₅₃H₆₄N₂O₂₂S

Guidance literature:: Multi-step reaction with 5 steps

1: 49 percent / N-iodosuccinimide; trifluoromethanesulfonic acid; molecular sieves 3 Angstroem / various solvent(s) / 5 h / -80 °C

2: 79 percent / pyridine; 4-dimethylaminopyridine / 42 h / 40 °C

3: trimethylamine / acetonitrile; H₂O / 48 h / 40 °C

4: 380 mg / potassium carbonate / dimethylformamide / 3 h / 20 °C

5: 94 percent / zinc / tetrahydrofuran / 28 h / 20 °C

With pyridine; dmap; N-iodo-succinimide; trifluorormethanesulfonic acid; 3 A molecular sieve; potassium carbonate; zinc; trimethylamine; In tetrahydrofuran; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/anie.200501608