bosentan potassium

Base Information

Chemical Name:bosentan potassium
CAS No.:1174918-31-0
Molecular Formula:C₂₇H₂₈N₅O₆S*K
Molecular Weight:589.714
Hs Code.:

Synonyms:bosentan potassium

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Chemical Property of bosentan potassium

Chemical Property:

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Technology Process of bosentan potassium

There total 6 articles about bosentan potassium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7388-28-5,10604-71-4,24768-69-2,26915-75-3,50856-01-4,92004-30-3
sodium 2-hydroxyethoxide

: 150727-06-3
4-tert-butyl-N-(6-chloro-5-(2-methoxyphenoxy)2,2'-bipyrimidin-4-yl)benzene sulfonamide

: 174227-14-6
p-tert-butyl-N-[6-hydroxy-5-(2-methoxyphenoxy)-2-(2-pyrimidinyl)-4-pyrimidinyl]benzenesulfonamide

: 1174918-31-0
bosentan potassium

Guidance literature:: sodium 2-hydroxyethoxide; 4-tert-butyl-N-(6-chloro-5-(2-methoxyphenoxy)2,2'-bipyrimidin-4-yl)benzene sulfonamide; In water; at 115 ℃; for 5h;

With potassium hydroxide; In water; isopropyl alcohol; at 55 - 85 ℃; for 1h;

Reference yield:

: 90-05-1
2-methoxy-phenol

: 1174918-31-0
bosentan potassium

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydroxide / toluene / 20 °C / Reflux

1.2: 3.5 h / 60 °C / Reflux

2.1: sodium ethanolate / methanol / 6 h / 0 - 35 °C

3.1: trichlorophosphate / 4 h / 103 - 105 °C

3.2: 20 - 80 °C

4.1: potassium carbonate / tetrabutylammomium bromide / toluene / 2 h / Reflux

5.1: water / 5 h / 115 °C

5.2: 1 h / 55 - 85 °C

With sodium ethanolate; potassium carbonate; sodium hydroxide; trichlorophosphate; tetrabutylammomium bromide; In methanol; water; toluene;

Reference yield:

: 150726-89-9
(2-methoxyphenoxy)-malonic acid dimethyl ester

: 1174918-31-0
bosentan potassium

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium ethanolate / methanol / 6 h / 0 - 35 °C

2.1: trichlorophosphate / 4 h / 103 - 105 °C

2.2: 20 - 80 °C

3.1: potassium carbonate / tetrabutylammomium bromide / toluene / 2 h / Reflux

4.1: water / 5 h / 115 °C

4.2: 1 h / 55 - 85 °C

With sodium ethanolate; potassium carbonate; trichlorophosphate; tetrabutylammomium bromide; In methanol; water; toluene;