C₄₄H₅₀O₁₁S

Base Information

Chemical Name:C₄₄H₅₀O₁₁S
CAS No.:482626-53-9
Molecular Formula:C₄₄H₅₀O₁₁S
Molecular Weight:786.94
Hs Code.:

C<sub>44</sub>H<sub>50</sub>O<sub>11</sub>S

Synonyms:C₄₄H₅₀O₁₁S

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Chemical Property of C₄₄H₅₀O₁₁S

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Technology Process of C₄₄H₅₀O₁₁S

There total 20 articles about C₄₄H₅₀O₁₁S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 76526-43-7
methyl 3,3-dimethoxy-2-methylpropionate

: 374752-87-1
C₃₉H₄₄O₉S

: 482626-53-9
C₄₄H₅₀O₁₁S

Guidance literature:: With toluene-4-sulfonic acid; In chloroform; for 12h; Heating;
DOI:10.1021/ja016272z

Reference yield: 68.0%

: 82387-42-6,143130-92-1,35588-82-0
methyl 3-methoxy-2-methyl-acrylate

: 76526-43-7
methyl 3,3-dimethoxy-2-methylpropionate

: 374752-87-1
C₃₉H₄₄O₉S

: 482626-53-9
C₄₄H₅₀O₁₁S

Guidance literature:: With toluene-4-sulfonic acid; In chloroform; for 12h; Heating;
DOI:10.1021/ja0279646

Reference yield:

: 482626-35-7
(2R,3S,4S,5S)-5-Benzyloxymethoxy-7-(4-methoxy-benzyloxy)-2,4-dimethyl-heptane-1,3-diol

: 482626-53-9
C₄₄H₅₀O₁₁S

Guidance literature:: Multi-step reaction with 13 steps

1: 100 percent / imidazole / CH₂Cl₂ / 1 h / 0 °C

2: 93 percent / NaHMDS / tetrahydrofuran; dimethylformamide / 1 h / 20 °C

3: 93 percent / tetrabutylammonium fluoride / tetrahydrofuran / 8 h / 20 °C

4: 96 percent / triethylamine; sulfur trioxide pyridine complex / dimethylsulfoxide; CH₂Cl₂ / 3 h / 20 °C

5: 99 percent / MgBr₂*Et₂O / CH₂Cl₂ / 3 h / 20 °C

6: osmium tetroxide; NMO / acetone; H₂O / 1.5 h / 20 °C

7: NaIO₄ / acetone; H₂O / 0.5 h / 20 °C

8: 3.24 g / NaBH₄ / ethanol / 0.5 h / 20 °C

9: 93 percent / pyridine; DMAP / CH₂Cl₂ / 24 h / 20 °C

10: 88 percent / CAN / acetonitrile; H₂O / 0.5 h / 20 °C

11: 99 percent / triethylamine / CH₂Cl₂ / 3 h / 0 °C

12: 99 percent / aq. HCl / acetonitrile / 2 h / 20 °C

13: 68 percent / p-TsOH*H₂O / CHCl₃ / 12 h / Heating

With pyridine; 1H-imidazole; hydrogenchloride; dmap; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; N-methyl-2-indolinone; ammonium cerium(IV) nitrate; tetrabutyl ammonium fluoride; sodium hexamethyldisilazane; sulfur trioxide pyridine complex; toluene-4-sulfonic acid; triethylamine; magnesium bromide; In tetrahydrofuran; ethanol; dichloromethane; chloroform; water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1021/ja0279646