dihydrido(2-methylamidopyridine-κ²-N,N′)bis(triphenylphosphine)iridium(III)

Base Information

• Chemical Name: dihydrido(2-methylamidopyridine-κ²-N,N′)bis(triphenylphosphine)iridium(III)
• CAS No.: 1396319-30-4
• Molecular Formula: C₄₂H₃₉IrN₂P₂
• Molecular Weight: 825.953

Synonyms:dihydrido(2-methylamidopyridine-κ²-N,N′)bis(triphenylphosphine)iridium(III)

Chemical Property of dihydrido(2-methylamidopyridine-κ²-N,N′)bis(triphenylphosphine)iridium(III)

Chemical Property:

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Technology Process of dihydrido(2-methylamidopyridine-κ²-N,N′)bis(triphenylphosphine)iridium(III)

There total 1 articles about dihydrido(2-methylamidopyridine-κ²-N,N′)bis(triphenylphosphine)iridium(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

2-(N-methylamino)pyridine (4597-87-9) + pentahydridobis(triphenylphosphine)iridium(III) (53470-69-2) → dihydrido(2-methylamidopyridine-κ2-N,N′)bis(triphenylphosphine)iridium(III) (1396319-30-4)

Guidance literature:

In benzene; at 65 ℃; for 21h; Inert atmosphere; Schlenk technique;

DOI:10.1021/ic300923c

Reference yield:

carbon dioxide (124-38-9,18923-20-1) + dihydrido(2-methylamidopyridine-κ2-N,N′)bis(triphenylphosphine)iridium(III) (1396319-30-4) → dihydrido(N-(2-methylpyridyl)carbamato-κ2-N′,O)bis(triphenylphosphine)iridium(III) (1396319-34-8)

Guidance literature:

In dichloromethane-d2; at 20 ℃; for 0.5h; Inert atmosphere; Schlenk technique;

DOI:10.1021/ic300923c

upstream raw materials:

2-(N-methylamino)pyridine

pentahydridobis(triphenylphosphine)iridium(III)

Downstream raw materials:

dihydrido(N-(2-methylpyridyl)carbamato-κ²-N′,O)bis(triphenylphosphine)iridium(III)

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