di-tert-butyl {[4'-(benzyloxy)-2',6'-dibromo-4-methoxy-(1,1'-biphenyl)-3,5-diyl]bis(methylene)}dicarbamate

Base Information

Chemical Name:di-tert-butyl {[4'-(benzyloxy)-2',6'-dibromo-4-methoxy-(1,1'-biphenyl)-3,5-diyl]bis(methylene)}dicarbamate
CAS No.:1262519-70-9
Molecular Formula:C₃₂H₃₈Br₂N₂O₆
Molecular Weight:706.472
Hs Code.:

Synonyms:di-tert-butyl {[4'-(benzyloxy)-2',6'-dibromo-4-methoxy-(1,1'-biphenyl)-3,5-diyl]bis(methylene)}dicarbamate

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Chemical Property of di-tert-butyl {[4'-(benzyloxy)-2',6'-dibromo-4-methoxy-(1,1'-biphenyl)-3,5-diyl]bis(methylene)}dicarbamate

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Technology Process of di-tert-butyl {[4'-(benzyloxy)-2',6'-dibromo-4-methoxy-(1,1'-biphenyl)-3,5-diyl]bis(methylene)}dicarbamate

There total 1 articles about di-tert-butyl {[4'-(benzyloxy)-2',6'-dibromo-4-methoxy-(1,1'-biphenyl)-3,5-diyl]bis(methylene)}dicarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1262519-64-1
2,6-bis[(N-tert-butyloxycarbonyl)aminomethyl]-4-(4',4',5',5'-tetramethyl-1',3',2'-dioxaborolan-2'-yl)anisole

: 556038-43-8
3,5-dibromo-4-iodophenol benzyl ether

: 1262519-70-9
di-tert-butyl {[4'-(benzyloxy)-2',6'-dibromo-4-methoxy-(1,1'-biphenyl)-3,5-diyl]bis(methylene)}dicarbamate

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In water; dimethyl sulfoxide; at 50 ℃; Inert atmosphere; Alkaline conditions;
DOI:10.1055/s-0030-1258238

Reference yield: 62.0%

: 1262519-70-9
di-tert-butyl {[4'-(benzyloxy)-2',6'-dibromo-4-methoxy-(1,1'-biphenyl)-3,5-diyl]bis(methylene)}dicarbamate

: 1066-54-2
trimethylsilylacetylene

: 1262519-74-3
di-tert-butyl {[4'-(benzyloxy)-4-methoxy-2',6'-bis(trimethylsilylethynyl)-(1,1'-biphenyl)-3,5-diyl]bis(methylene)}dicarbamate

Guidance literature:: With piperidine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; at 80 ℃; Inert atmosphere;
DOI:10.1055/s-0030-1258238