5-(1-benzyl-2-((triisopropylsilyl)oxy)-1H-indol-3-yl)-2-(benzyloxy)pentanenitrile

Base Information

Chemical Name:5-(1-benzyl-2-((triisopropylsilyl)oxy)-1H-indol-3-yl)-2-(benzyloxy)pentanenitrile
CAS No.:1254982-29-0
Molecular Formula:C₃₆H₄₆N₂O₂Si
Molecular Weight:566.859
Hs Code.:

Synonyms:5-(1-benzyl-2-((triisopropylsilyl)oxy)-1H-indol-3-yl)-2-(benzyloxy)pentanenitrile

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Chemical Property of 5-(1-benzyl-2-((triisopropylsilyl)oxy)-1H-indol-3-yl)-2-(benzyloxy)pentanenitrile

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Technology Process of 5-(1-benzyl-2-((triisopropylsilyl)oxy)-1H-indol-3-yl)-2-(benzyloxy)pentanenitrile

There total 6 articles about 5-(1-benzyl-2-((triisopropylsilyl)oxy)-1H-indol-3-yl)-2-(benzyloxy)pentanenitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: C₂₇H₂₆N₂O₂

: 1254982-29-0
5-(1-benzyl-2-((triisopropylsilyl)oxy)-1H-indol-3-yl)-2-(benzyloxy)pentanenitrile

Guidance literature:: With triisopropylsilyl trifluoromethanesulfonate; triethylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol102246d

Reference yield: 95.0%

: 1254982-27-8
5-(1-benzyl-1H-indol-3-yl)-2-(benzyloxy)pentanenitrile

: 80522-42-5
triisopropylsilyl trifluoromethanesulfonate

: 1254982-29-0
5-(1-benzyl-2-((triisopropylsilyl)oxy)-1H-indol-3-yl)-2-(benzyloxy)pentanenitrile

Guidance literature:: 5-(1-benzyl-1H-indol-3-yl)-2-(benzyloxy)pentanenitrile; With hydrogenchloride; In dimethyl sulfoxide; Inert atmosphere;

triisopropylsilyl trifluoromethanesulfonate; With triethylamine;
DOI:10.1021/co4000387

Reference yield:

: 17206-61-0
hept-6-enal

: 1254982-29-0
5-(1-benzyl-2-((triisopropylsilyl)oxy)-1H-indol-3-yl)-2-(benzyloxy)pentanenitrile

Guidance literature:: Multi-step reaction with 4 steps

1.1: bismuth(III) bromide / dichloromethane / Inert atmosphere

1.2: Inert atmosphere

2.1: ozone / dichloromethane / Inert atmosphere

2.2: Inert atmosphere

3.1: acetic acid / Heating

4.1: hydrogenchloride / dimethyl sulfoxide / Inert atmosphere

With hydrogenchloride; bismuth(III) bromide; ozone; acetic acid; In dichloromethane; dimethyl sulfoxide;
DOI:10.1021/co4000387