ethyl DL-2,4-bis<(benzoylthio)acetamido>butanoate

Base Information

Chemical Name:ethyl DL-2,4-bis<(benzoylthio)acetamido>butanoate
CAS No.:103668-22-0
Molecular Formula:C₂₄H₂₆N₂O₆S₂
Molecular Weight:502.612
Hs Code.:

Synonyms:ethyl DL-2,4-bis<(benzoylthio)acetamido>butanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl DL-2,4-bis<(benzoylthio)acetamido>butanoate

Chemical Property:

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Technology Process of ethyl DL-2,4-bis<(benzoylthio)acetamido>butanoate

There total 2 articles about ethyl DL-2,4-bis<(benzoylthio)acetamido>butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 28170-13-0
thiobenzoic acid potassium salt

: 103668-09-3
ethyl DL-2,4-bis(chloroacetamido)butanoate

: 103668-22-0
ethyl DL-2,4-bis<(benzoylthio)acetamido>butanoate

Guidance literature:: In ethanol; for 3h; Heating;
DOI:10.1021/jm00160a023

Reference yield:

: 103668-08-2
2,4-diaminobutyrate ethyl ester dihydrochloride

: 103668-22-0
ethyl DL-2,4-bis<(benzoylthio)acetamido>butanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / NaHCO₃ / toluene; H₂O / 15 h / Ambient temperature

2: 95 percent / ethanol / 3 h / Heating

With sodium hydrogencarbonate; In ethanol; water; toluene;
DOI:10.1021/jm00160a023