2-(tert-butyldiphenylsiloxymethyl)-5-methyl-2(E),5-dienoic acid N-(2-iodophenyl)amide

Base Information

Chemical Name:2-(tert-butyldiphenylsiloxymethyl)-5-methyl-2(E),5-dienoic acid N-(2-iodophenyl)amide
CAS No.:328093-35-2
Molecular Formula:C₃₀H₃₄INO₂Si
Molecular Weight:595.595
Hs Code.:

Synonyms:2-(tert-butyldiphenylsiloxymethyl)-5-methyl-2(E),5-dienoic acid N-(2-iodophenyl)amide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(tert-butyldiphenylsiloxymethyl)-5-methyl-2(E),5-dienoic acid N-(2-iodophenyl)amide

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Technology Process of 2-(tert-butyldiphenylsiloxymethyl)-5-methyl-2(E),5-dienoic acid N-(2-iodophenyl)amide

There total 6 articles about 2-(tert-butyldiphenylsiloxymethyl)-5-methyl-2(E),5-dienoic acid N-(2-iodophenyl)amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 615-43-0
2-iodophenylamine

: 2-(tert-butyldiphenylsiloxymethyl)-5-methyl-2(E),5-dienoic acid

: 328093-35-2
2-(tert-butyldiphenylsiloxymethyl)-5-methyl-2(E),5-dienoic acid N-(2-iodophenyl)amide

Guidance literature:: With 2-chloro-1-methyl-pyridinium iodide; In toluene; at 80 ℃; for 4h;
DOI:10.1016/j.tet.2010.05.048

Reference yield:

: 148901-34-2
methyl 3-hydroxy-5-methyl-2-methylene-4-hexenoate

: 328093-35-2
2-(tert-butyldiphenylsiloxymethyl)-5-methyl-2(E),5-dienoic acid N-(2-iodophenyl)amide

Guidance literature:: Multi-step reaction with 6 steps

1: pyridine

2: MgBr₂*OEt₂

3: DIEA

4: LiOH

5: 1-methyl-2-chloropyridinium iodide

With pyridine; lithium hydroxide; 2-chloro-1-methyl-pyridinium iodide; N-ethyl-N,N-diisopropylamine; magnesium bromide;
DOI:10.1002/1521-3773(20001215)39:24<4596::AID-ANIE4596>3.0.CO;2-F

Reference yield:

: (Z)-2-Bromomethyl-5-methyl-hexa-2,4-dienoic acid methyl ester

: 328093-35-2
2-(tert-butyldiphenylsiloxymethyl)-5-methyl-2(E),5-dienoic acid N-(2-iodophenyl)amide

Guidance literature:: Multi-step reaction with 4 steps

1: DIEA

2: LiOH

3: 1-methyl-2-chloropyridinium iodide

With lithium hydroxide; 2-chloro-1-methyl-pyridinium iodide; N-ethyl-N,N-diisopropylamine;
DOI:10.1002/1521-3773(20001215)39:24<4596::AID-ANIE4596>3.0.CO;2-F