Diethyl-carbamic acid (1R,6S)-6-((R)-1-hydroxy-1,5-dimethyl-hex-4-enyl)-cyclohex-2-enyl ester

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Chemical Name:Diethyl-carbamic acid (1R,6S)-6-((R)-1-hydroxy-1,5-dimethyl-hex-4-enyl)-cyclohex-2-enyl ester
CAS No.:129436-61-9
Molecular Formula:C₁₉H₃₃NO₃
Molecular Weight:323.476
Hs Code.:

Synonyms:Diethyl-carbamic acid (1R,6S)-6-((R)-1-hydroxy-1,5-dimethyl-hex-4-enyl)-cyclohex-2-enyl ester

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Chemical Property of Diethyl-carbamic acid (1R,6S)-6-((R)-1-hydroxy-1,5-dimethyl-hex-4-enyl)-cyclohex-2-enyl ester

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Technology Process of Diethyl-carbamic acid (1R,6S)-6-((R)-1-hydroxy-1,5-dimethyl-hex-4-enyl)-cyclohex-2-enyl ester

There total 1 articles about Diethyl-carbamic acid (1R,6S)-6-((R)-1-hydroxy-1,5-dimethyl-hex-4-enyl)-cyclohex-2-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 37586-57-5
4-methyl-3-pentenylmagnesium bromide

: 129436-54-0
Diethyl-carbamic acid (1S,6R)-6-acetyl-3-methyl-cyclohex-2-enyl ester

: 129436-61-9
Diethyl-carbamic acid (1R,6S)-6-((R)-1-hydroxy-1,5-dimethyl-hex-4-enyl)-cyclohex-2-enyl ester

Guidance literature:: In tetrahydrofuran; at 0 ℃;
DOI:10.1016/S0040-4039(00)88818-8

Reference yield: 100.0%

: 129436-61-9
Diethyl-carbamic acid (1R,6S)-6-((R)-1-hydroxy-1,5-dimethyl-hex-4-enyl)-cyclohex-2-enyl ester

: 129436-62-0
(1R,6S)-6-((R)-1-Hydroxy-1,5-dimethyl-hex-4-enyl)-cyclohex-2-enol

Guidance literature:: With lithium aluminium tetrahydride;
DOI:10.1016/S0040-4039(00)88818-8

Reference yield:

: 129436-61-9
Diethyl-carbamic acid (1R,6S)-6-((R)-1-hydroxy-1,5-dimethyl-hex-4-enyl)-cyclohex-2-enyl ester

: 115655-93-1
(R)-6-((R)-1-Hydroxy-1,5-dimethyl-hex-4-enyl)-cyclohex-2-enone

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / LiAlH₄

2: 48 percent / MnO₂ / CH₂Cl₂

With manganese(IV) oxide; lithium aluminium tetrahydride; In dichloromethane;
DOI:10.1016/S0040-4039(00)88818-8