C₃₁H₃₂ClN₉O₆S

Base Information

• Chemical Name: C₃₁H₃₂ClN₉O₆S
• CAS No.: 1407155-93-4
• Molecular Formula: C₃₁H₃₂ClN₉O₆S
• Molecular Weight: 694.171
• Mol file: 1407155-93-4.mol

Synonyms:C₃₁H₃₂ClN₉O₆S

Chemical Property of C₃₁H₃₂ClN₉O₆S

Chemical Property:

Purity/Quality:

Safty Information:

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• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₁H₃₂ClN₉O₆S

There total 8 articles about C₃₁H₃₂ClN₉O₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

C16H17ClN6O2S (1407155-68-3) + R-2-<(4-ethyl-2,3-dioxo-1-piperadinyl)formamido> phenylacetyl chloride (64205-06-7) → C31H32ClN9O6S (1407155-93-4)

Guidance literature:

With pyridine; In dichloromethane; at -40 - -30 ℃; for 1h;

Reference yield:

C20H22N6O5S (1407155-66-1) → C31H32ClN9O6S (1407155-93-4)

Guidance literature:

Multi-step reaction with 3 steps

1: pyridine; bis(trichloromethyl) carbonate / dichloromethane / 2 h / Cooling with ice

2: dimedone; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / dichloromethane / 1 h / 20 °C

3: pyridine / dichloromethane / 1 h / -40 - -30 °C

With pyridine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; bis(trichloromethyl) carbonate; dimedone; In dichloromethane;

Reference yield:

C22H24N6O6S (1407155-65-0) → C31H32ClN9O6S (1407155-93-4)

Guidance literature:

Multi-step reaction with 4 steps

1: sulfuric acid / water; tetrahydrofuran / 3 h / 45 °C

2: pyridine; bis(trichloromethyl) carbonate / dichloromethane / 2 h / Cooling with ice

3: dimedone; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / dichloromethane / 1 h / 20 °C

4: pyridine / dichloromethane / 1 h / -40 - -30 °C

With pyridine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; bis(trichloromethyl) carbonate; sulfuric acid; dimedone; In tetrahydrofuran; dichloromethane; water;

upstream raw materials:

C₂₂H₂₄N₆O₆S

C₂₀H₂₂N₆O₅S

C₂₀H₂₁ClN₆O₄S

C₁₆H₁₇ClN₆O₂S