2-<2-<2-methanesulfonyloxy-3-(octadecyloxy)propyloxy>ethoxy>ethyl trityl ether

Base Information

Chemical Name:2-<2-<2-methanesulfonyloxy-3-(octadecyloxy)propyloxy>ethoxy>ethyl trityl ether
CAS No.:115734-60-6
Molecular Formula:C₄₅H₆₈O₇S
Molecular Weight:753.097
Hs Code.:

Synonyms:2-<2-<2-methanesulfonyloxy-3-(octadecyloxy)propyloxy>ethoxy>ethyl trityl ether

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Chemical Property of 2-<2-<2-methanesulfonyloxy-3-(octadecyloxy)propyloxy>ethoxy>ethyl trityl ether

Chemical Property:

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Technology Process of 2-<2-<2-methanesulfonyloxy-3-(octadecyloxy)propyloxy>ethoxy>ethyl trityl ether

There total 8 articles about 2-<2-<2-methanesulfonyloxy-3-(octadecyloxy)propyloxy>ethoxy>ethyl trityl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 124-63-0
methanesulfonyl chloride

: 115733-85-2
2-<2-<2-hydroxy-3-(octadecyloxy)propyloxy>ethoxy>ethyl trityl ether

: 115734-60-6
2-<2-<2-methanesulfonyloxy-3-(octadecyloxy)propyloxy>ethoxy>ethyl trityl ether

Guidance literature:: With triethylamine; In dichloromethane; for 1.5h; ice-cooling;
DOI:10.1248/cpb.37.3277

Reference yield:

: 544-62-7
batyl alcohol

: 115734-60-6
2-<2-<2-methanesulfonyloxy-3-(octadecyloxy)propyloxy>ethoxy>ethyl trityl ether

Guidance literature:: Multi-step reaction with 4 steps

1: 55 percent / pyridine / CH₂Cl₂ / 48 h / Ambient temperature

2: 60percent NaH (in mineral oil) / dioxane / room temperature, 1 h, 90 deg C, 13 h

3: pyridine / 15 h / 40 °C

4: 71 percent / Et₃N / CH₂Cl₂ / 1.5 h / ice-cooling

With pyridine; sodium hydride; triethylamine; In 1,4-dioxane; pyridine; dichloromethane;
DOI:10.1248/cpb.37.3277

Reference yield:

: 86541-07-3
2-hydroxy-3-(octadecyloxy)propyl p-toluenesulfonate

: 115734-60-6
2-<2-<2-methanesulfonyloxy-3-(octadecyloxy)propyloxy>ethoxy>ethyl trityl ether

Guidance literature:: Multi-step reaction with 3 steps

1: 60percent NaH (in mineral oil) / dioxane / room temperature, 1 h, 90 deg C, 13 h

2: pyridine / 15 h / 40 °C

3: 71 percent / Et₃N / CH₂Cl₂ / 1.5 h / ice-cooling

With sodium hydride; triethylamine; In 1,4-dioxane; pyridine; dichloromethane;
DOI:10.1248/cpb.37.3277