4-methoxyphenyl 2-acetamido-4-O-acetyl-3,6-di-O-benzoyl-2-deoxy-β-D-galacto-pyranoside

Base Information

Chemical Name:4-methoxyphenyl 2-acetamido-4-O-acetyl-3,6-di-O-benzoyl-2-deoxy-β-D-galacto-pyranoside
CAS No.:1164151-26-1
Molecular Formula:C₃₁H₃₁NO₁₀
Molecular Weight:577.588
Hs Code.:

Synonyms:4-methoxyphenyl 2-acetamido-4-O-acetyl-3,6-di-O-benzoyl-2-deoxy-β-D-galacto-pyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-methoxyphenyl 2-acetamido-4-O-acetyl-3,6-di-O-benzoyl-2-deoxy-β-D-galacto-pyranoside

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Technology Process of 4-methoxyphenyl 2-acetamido-4-O-acetyl-3,6-di-O-benzoyl-2-deoxy-β-D-galacto-pyranoside

There total 1 articles about 4-methoxyphenyl 2-acetamido-4-O-acetyl-3,6-di-O-benzoyl-2-deoxy-β-D-galacto-pyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1164151-25-0
4-methoxyphenyl 2-acetamido-3,6-di-O-benzoyl-2-deoxy-β-D-galactopyranoside

: 108-24-7
acetic anhydride

: 1164151-26-1
4-methoxyphenyl 2-acetamido-4-O-acetyl-3,6-di-O-benzoyl-2-deoxy-β-D-galacto-pyranoside

Guidance literature:: With pyridine; at 0 - 20 ℃; for 24h; Inert atmosphere;
DOI:10.1016/j.tet.2009.03.067

Reference yield: 79.0%

: 1164151-26-1
4-methoxyphenyl 2-acetamido-4-O-acetyl-3,6-di-O-benzoyl-2-deoxy-β-D-galacto-pyranoside

: 108-98-5
thiophenol

: 1164151-27-2
phenyl 2-acetamido-4-O-acetyl-3,6-di-O-benzoyl-2-deoxy-1-thio-β-D-galactopyranoside

Guidance literature:: With boron trifluoride diethyl etherate; In chloroform; at 60 ℃; for 24h; Inert atmosphere; Molecular sieve;
DOI:10.1016/j.tet.2009.03.067

Reference yield: 68.0%

: 1122-97-0
4-methylsulfanyl-thiophenol

: 1164151-26-1
4-methoxyphenyl 2-acetamido-4-O-acetyl-3,6-di-O-benzoyl-2-deoxy-β-D-galacto-pyranoside

: 1164151-28-3
4-methylthiophenyl 2-acetamido-4-O-acetyl-3,6-di-O-benzoyl-2-deoxy-1-thio-β-D-galactopyranoside

Guidance literature:: With boron trifluoride diethyl etherate; In chloroform; at 60 ℃; for 24h; Inert atmosphere; Molecular sieve;
DOI:10.1016/j.tet.2009.03.067