2-[2-(2-{5-{2-[2-(2-hydroxy-ethoxy)-ethoxy]-ethylsulfanyl}-2-[5-(toluene-4-sulfonyl)-5H-[1,3]dithiolo[4,5-c]pyrrol-2-ylidene]-[1,3]dithiol-4-ylsulfanyl}-ethoxy)-ethoxy]-ethanol

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Chemical Name:2-[2-(2-{5-{2-[2-(2-hydroxy-ethoxy)-ethoxy]-ethylsulfanyl}-2-[5-(toluene-4-sulfonyl)-5H-[1,3]dithiolo[4,5-c]pyrrol-2-ylidene]-[1,3]dithiol-4-ylsulfanyl}-ethoxy)-ethoxy]-ethanol
CAS No.:487048-99-7
Molecular Formula:C₂₇H₃₅NO₈S₇
Molecular Weight:726.039
Hs Code.:
Mol file:487048-99-7.mol

2-[2-(2-{5-{2-[2-(2-hydroxy-ethoxy)-ethoxy]-ethylsulfanyl}-2-[5-(toluene-4-sulfonyl)-5<i>H</i>-[1,3]dithiolo[4,5-<i>c</i>]pyrrol-2-ylidene]-[1,3]dithiol-4-ylsulfanyl}-ethoxy)-ethoxy]-ethanol

Synonyms:2-[2-(2-{5-{2-[2-(2-hydroxy-ethoxy)-ethoxy]-ethylsulfanyl}-2-[5-(toluene-4-sulfonyl)-5H-[1,3]dithiolo[4,5-c]pyrrol-2-ylidene]-[1,3]dithiol-4-ylsulfanyl}-ethoxy)-ethoxy]-ethanol

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Chemical Property of 2-[2-(2-{5-{2-[2-(2-hydroxy-ethoxy)-ethoxy]-ethylsulfanyl}-2-[5-(toluene-4-sulfonyl)-5H-[1,3]dithiolo[4,5-c]pyrrol-2-ylidene]-[1,3]dithiol-4-ylsulfanyl}-ethoxy)-ethoxy]-ethanol Edit

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Technology Process of 2-[2-(2-{5-{2-[2-(2-hydroxy-ethoxy)-ethoxy]-ethylsulfanyl}-2-[5-(toluene-4-sulfonyl)-5H-[1,3]dithiolo[4,5-c]pyrrol-2-ylidene]-[1,3]dithiol-4-ylsulfanyl}-ethoxy)-ethoxy]-ethanol

There total 2 articles about 2-[2-(2-{5-{2-[2-(2-hydroxy-ethoxy)-ethoxy]-ethylsulfanyl}-2-[5-(toluene-4-sulfonyl)-5H-[1,3]dithiolo[4,5-c]pyrrol-2-ylidene]-[1,3]dithiol-4-ylsulfanyl}-ethoxy)-ethoxy]-ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 62573-16-4
2-[2-(2-iodoethoxy)ethoxy]ethanol

: 3-{5-{2-[2-(2-hydroxy-ethoxy)-ethoxy]-ethylsulfanyl}-2-[5-(toluene-4-sulfonyl)-5H-[1,3]dithiolo[4,5-c]pyrrol-2-ylidene]-[1,3]dithiol-4-ylsulfanyl}-propionitrile

: 487048-99-7
2-[2-(2-{5-{2-[2-(2-hydroxy-ethoxy)-ethoxy]-ethylsulfanyl}-2-[5-(toluene-4-sulfonyl)-5H-[1,3]dithiolo[4,5-c]pyrrol-2-ylidene]-[1,3]dithiol-4-ylsulfanyl}-ethoxy)-ethoxy]-ethanol

Guidance literature:: 3-{5-{2-[2-(2-hydroxy-ethoxy)-ethoxy]-ethylsulfanyl}-2-[5-(toluene-4-sulfonyl)-5H-[1,3]dithiolo[4,5-c]pyrrol-2-ylidene]-[1,3]dithiol-4-ylsulfanyl}-propionitrile; With cesium hydroxide; In tetrahydrofuran;

2-[2-(2-iodoethoxy)ethoxy]ethanol; In tetrahydrofuran; at 20 ℃; for 1h; Further stages.;
DOI:10.1021/ol026816h

Reference yield:

: 300766-20-5
N-tosyl-2-(4,5-bis(2-cyanoethylthio)-(1,3)-dithiole-2-ylidene)-(1,3)-dithiolo[4,5-c]pyrrole

: 487048-99-7
2-[2-(2-{5-{2-[2-(2-hydroxy-ethoxy)-ethoxy]-ethylsulfanyl}-2-[5-(toluene-4-sulfonyl)-5H-[1,3]dithiolo[4,5-c]pyrrol-2-ylidene]-[1,3]dithiol-4-ylsulfanyl}-ethoxy)-ethoxy]-ethanol

Guidance literature:: Multi-step reaction with 2 steps

1.1: CsOH*H₂O / tetrahydrofuran

1.2: tetrahydrofuran / 1 h / 20 °C

2.1: CsOH*H₂O / tetrahydrofuran

2.2: tetrahydrofuran / 1 h / 20 °C

With cesium hydroxide; In tetrahydrofuran;
DOI:10.1021/ol026816h