C₃₃H₆₂O₇SSi₂

Base Information

Chemical Name:C₃₃H₆₂O₇SSi₂
CAS No.:1265902-72-4
Molecular Formula:C₃₃H₆₂O₇SSi₂
Molecular Weight:659.088
Hs Code.:

C<sub>33</sub>H<sub>62</sub>O<sub>7</sub>SSi<sub>2</sub>

Synonyms:C₃₃H₆₂O₇SSi₂

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Chemical Property of C₃₃H₆₂O₇SSi₂

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Technology Process of C₃₃H₆₂O₇SSi₂

There total 4 articles about C₃₃H₆₂O₇SSi₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1265902-71-3
C₂₆H₅₆O₅Si₂

: 98-59-9
p-toluenesulfonyl chloride

: 1265902-72-4
C₃₃H₆₂O₇SSi₂

Guidance literature:: With pyridine; at 0 ℃; for 48h; Inert atmosphere;
DOI:10.1021/ol1029657

Reference yield:

: 994-30-9
triethylsilyl chloride

: 1265902-72-4
C₃₃H₆₂O₇SSi₂

Guidance literature:: Multi-step reaction with 3 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

2: palladium 10% on activated carbon; hydrogen / ethanol / 11 h / 30 °C

3: pyridine / 48 h / 0 °C / Inert atmosphere

With pyridine; 1H-imidazole; palladium 10% on activated carbon; hydrogen; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/ol1029657

Reference yield:

: 1265902-70-2
C₃₃H₆₂O₅Si₂

: 1265902-72-4
C₃₃H₆₂O₇SSi₂

Guidance literature:: Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen / ethanol / 11 h / 30 °C

2: pyridine / 48 h / 0 °C / Inert atmosphere

With pyridine; palladium 10% on activated carbon; hydrogen; In ethanol;
DOI:10.1021/ol1029657