[(2S,6S)-2-(tert-Butyl-diphenyl-silanyloxymethyl)-4-(dimethoxy-phosphoryloxy)-6-methoxy-6H-pyran-(3E)-ylidene]-acetic acid methyl ester

Base Information

Chemical Name:[(2S,6S)-2-(tert-Butyl-diphenyl-silanyloxymethyl)-4-(dimethoxy-phosphoryloxy)-6-methoxy-6H-pyran-(3E)-ylidene]-acetic acid methyl ester
CAS No.:191729-47-2
Molecular Formula:C₂₈H₃₇O₉PSi
Molecular Weight:576.656
Hs Code.:

Synonyms:[(2S,6S)-2-(tert-Butyl-diphenyl-silanyloxymethyl)-4-(dimethoxy-phosphoryloxy)-6-methoxy-6H-pyran-(3E)-ylidene]-acetic acid methyl ester

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Chemical Property of [(2S,6S)-2-(tert-Butyl-diphenyl-silanyloxymethyl)-4-(dimethoxy-phosphoryloxy)-6-methoxy-6H-pyran-(3E)-ylidene]-acetic acid methyl ester

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Technology Process of [(2S,6S)-2-(tert-Butyl-diphenyl-silanyloxymethyl)-4-(dimethoxy-phosphoryloxy)-6-methoxy-6H-pyran-(3E)-ylidene]-acetic acid methyl ester

There total 1 articles about [(2S,6S)-2-(tert-Butyl-diphenyl-silanyloxymethyl)-4-(dimethoxy-phosphoryloxy)-6-methoxy-6H-pyran-(3E)-ylidene]-acetic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 5927-18-4
trimethyl phosphonoacetate

: Benzoic acid (2R,6S)-2-(tert-butyl-diphenyl-silanyloxymethyl)-6-methoxy-3-oxo-3,6-dihydro-2H-pyran-4-yl ester

: 191729-47-2
[(2S,6S)-2-(tert-Butyl-diphenyl-silanyloxymethyl)-4-(dimethoxy-phosphoryloxy)-6-methoxy-6H-pyran-(3E)-ylidene]-acetic acid methyl ester

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; toluene;
DOI:10.1016/S0040-4020(97)00425-0

Reference yield: 77.0%

: 191729-47-2
[(2S,6S)-2-(tert-Butyl-diphenyl-silanyloxymethyl)-4-(dimethoxy-phosphoryloxy)-6-methoxy-6H-pyran-(3E)-ylidene]-acetic acid methyl ester

: methyl 6-O-(tert-butyldiphenyl)silyl-2,4-dideoxy-4-C-<(methoxycarbonyl)methyl>-3-O-(dimethoxyphosphoryl)-α-D-glycero-hex-3-enopyranoside

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; ethyl acetate; for 3h; under 2625.21 Torr; Ambient temperature; other catalysts and solvent;
DOI:10.1080/07328309908543975

Reference yield: 25.0%

: 191729-47-2
[(2S,6S)-2-(tert-Butyl-diphenyl-silanyloxymethyl)-4-(dimethoxy-phosphoryloxy)-6-methoxy-6H-pyran-(3E)-ylidene]-acetic acid methyl ester

: methyl 6-O-(tert-butyldiphenyl)silyl-2,4-dideoxy-4-C-<(methoxycarbonyl)methyl>-3-O-(dimethoxyphosphoryl)-α-D-lyxo-hexopyranoside

: methyl 6-O-(tert-butyldiphenyl)silyl-2,4-dideoxy-4-C-<(methoxycarbonyl)methyl>-3-O-(dimethoxyphosphoryl)-α-D-glycero-hex-3-enopyranoside

Guidance literature:: With hydrogen; W-7 Raney Nickel; In methanol; for 8h; under 2497.7 Torr; Ambient temperature;
DOI:10.1080/07328309908543975