Technology Process of C15H10Br2Cl2N2O2
There total 4 articles about C15H10Br2Cl2N2O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: phosphorus pentachloride; trichlorophosphate / 5 h / 70 - 140 °C
2: dipotassium hydrogenphosphate / tetrakis(triphenylphosphine) palladium(0) / DMF (N,N-dimethyl-formamide); water / 21 h / 68 °C
3: hydrogenchloride; iron / ethanol; water / 2 h / 90 °C
4: bromine; acetic acid / 23 h / 20 °C
5: methanesulfonic acid / 130 °C
With
hydrogenchloride; dipotassium hydrogenphosphate; methanesulfonic acid; phosphorus pentachloride; bromine; iron; acetic acid; trichlorophosphate;
tetrakis(triphenylphosphine) palladium(0);
In
DMF (N,N-dimethyl-formamide); ethanol; water;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: dipotassium hydrogenphosphate / tetrakis(triphenylphosphine) palladium(0) / DMF (N,N-dimethyl-formamide); water / 21 h / 68 °C
2: hydrogenchloride; iron / ethanol; water / 2 h / 90 °C
3: bromine; acetic acid / 23 h / 20 °C
4: methanesulfonic acid / 130 °C
With
hydrogenchloride; dipotassium hydrogenphosphate; methanesulfonic acid; bromine; iron; acetic acid;
tetrakis(triphenylphosphine) palladium(0);
In
DMF (N,N-dimethyl-formamide); ethanol; water;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: hydrogenchloride; iron / ethanol; water / 2 h / 90 °C
2: bromine; acetic acid / 23 h / 20 °C
3: methanesulfonic acid / 130 °C
With
hydrogenchloride; methanesulfonic acid; bromine; iron; acetic acid;
In
ethanol; water;