Technology Process of C27H37N3O6
There total 8 articles about C27H37N3O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1: diethyl ether; CH2Cl2 / -5 - 20 °C
2: 99 percent / AgOBz; Et3N / -25 - 20 °C
3: 1,2,4-triazole / CH2Cl2 / 0 - 20 °C
4: BF3*Et2O / CH2Cl2; diethyl ether
5: NaOH / methanol; tetrahydrofuran
6: diphenyl phosphoryl azide; Et3N / toluene / Heating
7: toluene / Heating
With
1,2,4-Triazole; sodium hydroxide; diphenyl phosphoryl azide; boron trifluoride diethyl etherate; silver benzoate; triethylamine;
In
tetrahydrofuran; methanol; diethyl ether; dichloromethane; toluene;
DOI:10.1016/j.bmcl.2006.06.090
- Guidance literature:
-
Multi-step reaction with 8 steps
1: SOCl2; DMF / CH2Cl2 / -10 - 20 °C
2: diethyl ether; CH2Cl2 / -5 - 20 °C
3: 99 percent / AgOBz; Et3N / -25 - 20 °C
4: 1,2,4-triazole / CH2Cl2 / 0 - 20 °C
5: BF3*Et2O / CH2Cl2; diethyl ether
6: NaOH / methanol; tetrahydrofuran
7: diphenyl phosphoryl azide; Et3N / toluene / Heating
8: toluene / Heating
With
1,2,4-Triazole; sodium hydroxide; thionyl chloride; diphenyl phosphoryl azide; boron trifluoride diethyl etherate; silver benzoate; triethylamine; N,N-dimethyl-formamide;
In
tetrahydrofuran; methanol; diethyl ether; dichloromethane; toluene;
DOI:10.1016/j.bmcl.2006.06.090
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1,2,4-triazole / CH2Cl2 / 0 - 20 °C
2: BF3*Et2O / CH2Cl2; diethyl ether
3: NaOH / methanol; tetrahydrofuran
4: diphenyl phosphoryl azide; Et3N / toluene / Heating
5: toluene / Heating
With
1,2,4-Triazole; sodium hydroxide; diphenyl phosphoryl azide; boron trifluoride diethyl etherate; triethylamine;
In
tetrahydrofuran; methanol; diethyl ether; dichloromethane; toluene;
DOI:10.1016/j.bmcl.2006.06.090