Benzyloxycarbonyl-S-(2,4,6-trimethylbenzyl)cysteinyl-tyrosyl-phenylalanine Methyl Ester

Base Information

Chemical Name:Benzyloxycarbonyl-S-(2,4,6-trimethylbenzyl)cysteinyl-tyrosyl-phenylalanine Methyl Ester
CAS No.:89137-78-0
Molecular Formula:C₄₀H₄₅N₃O₇S
Molecular Weight:711.879
Hs Code.:

Synonyms:Benzyloxycarbonyl-S-(2,4,6-trimethylbenzyl)cysteinyl-tyrosyl-phenylalanine Methyl Ester

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Chemical Property of Benzyloxycarbonyl-S-(2,4,6-trimethylbenzyl)cysteinyl-tyrosyl-phenylalanine Methyl Ester

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Technology Process of Benzyloxycarbonyl-S-(2,4,6-trimethylbenzyl)cysteinyl-tyrosyl-phenylalanine Methyl Ester

There total 5 articles about Benzyloxycarbonyl-S-(2,4,6-trimethylbenzyl)cysteinyl-tyrosyl-phenylalanine Methyl Ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3417-91-2
L-tyrosine methyl ester HCl

: 89137-78-0
Benzyloxycarbonyl-S-(2,4,6-trimethylbenzyl)cysteinyl-tyrosyl-phenylalanine Methyl Ester

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / 1-Hydroxybenzotriazole, N-Ethylpiperidine, N,N'-Dicyclohexylcarbodiimide / dimethylformamide; ethyl acetate / 1)1 h stirring at -5 deg C, 2)12 h at room temperature

2: 95 percent / NaOH / methanol; H₂O / 1 h / Ambient temperature

3: 1)Dicyclohexylcarbodiimide, 1-Hydroxybenztriazole, 1)Triethylamine / 1) DMF, -5 to -10 deg C, 1 h 2) Room temperature, 2 h

With 1-ethyl-piperidine; sodium hydroxide; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In methanol; water; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1135/cccc19832862

Reference yield:

: 89137-75-7
Benzyloxycarbonyl-S-(2,4,6-trimethylbenzyl)cysteinyl-tyrosine Methyl Ester

: 89137-78-0
Benzyloxycarbonyl-S-(2,4,6-trimethylbenzyl)cysteinyl-tyrosyl-phenylalanine Methyl Ester

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / NaOH / methanol; H₂O / 1 h / Ambient temperature

2: 1)Dicyclohexylcarbodiimide, 1-Hydroxybenztriazole, 1)Triethylamine / 1) DMF, -5 to -10 deg C, 1 h 2) Room temperature, 2 h

With sodium hydroxide; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In methanol; water;
DOI:10.1135/cccc19832862

Reference yield:

: 78221-56-4
N-benzyloxycarbonyl-S-(2,4,6-trimethylbenzyl)-L-cysteine

: 89137-78-0
Benzyloxycarbonyl-S-(2,4,6-trimethylbenzyl)cysteinyl-tyrosyl-phenylalanine Methyl Ester

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / 1-Hydroxybenzotriazole, N-Ethylpiperidine, N,N'-Dicyclohexylcarbodiimide / dimethylformamide; ethyl acetate / 1)1 h stirring at -5 deg C, 2)12 h at room temperature

2: 95 percent / NaOH / methanol; H₂O / 1 h / Ambient temperature

3: 1)Dicyclohexylcarbodiimide, 1-Hydroxybenztriazole, 1)Triethylamine / 1) DMF, -5 to -10 deg C, 1 h 2) Room temperature, 2 h

With 1-ethyl-piperidine; sodium hydroxide; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In methanol; water; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1135/cccc19832862