C₂₃H₂₀N₂O₅

Base Information

Chemical Name:C₂₃H₂₀N₂O₅
CAS No.:1177423-30-1
Molecular Formula:C₂₃H₂₀N₂O₅
Molecular Weight:404.422
Hs Code.:

C<sub>23</sub>H<sub>20</sub>N<sub>2</sub>O<sub>5</sub>

Synonyms:C₂₃H₂₀N₂O₅

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Chemical Property of C₂₃H₂₀N₂O₅

Chemical Property:

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Technology Process of C₂₃H₂₀N₂O₅

There total 8 articles about C₂₃H₂₀N₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 88912-27-0
3-chloro-isonicotinic acid

: 1177423-30-1
C₂₃H₂₀N₂O₅

Guidance literature:: Multi-step reaction with 7 steps

1.1: potassium carbonate / dimethyl sulfoxide / 0.5 h

1.2: 2 h / 20 °C

2.1: n-butyllithium; diisopropylamine / tetrahydrofuran; hexane / 1 h / -78 °C

2.2: 1 h / -78 °C

3.1: acetic acid / N,N-dimethyl-formamide / 62 h / 140 °C

4.1: sodium tetrahydroborate / methanol; dichloromethane / 3 h / 0 °C

5.1: dmap / dichloromethane / 0 - 20 °C

6.1: titanium tetrachloride / dichloromethane / 0.08 h / 0 °C

6.2: 1 h / 0 °C

7.1: water; sodium hydroxide / tetrahydrofuran; methanol; dichloromethane / 4 h / 20 °C

With dmap; sodium tetrahydroborate; n-butyllithium; water; titanium tetrachloride; potassium carbonate; acetic acid; diisopropylamine; sodium hydroxide; In tetrahydrofuran; methanol; hexane; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;

Reference yield:

: 98273-79-1
3-chloropyridine-4-carboxylic acid methyl ester

: 1177423-30-1
C₂₃H₂₀N₂O₅

Guidance literature:: Multi-step reaction with 6 steps

1.1: n-butyllithium; diisopropylamine / tetrahydrofuran; hexane / 1 h / -78 °C

1.2: 1 h / -78 °C

2.1: acetic acid / N,N-dimethyl-formamide / 62 h / 140 °C

3.1: sodium tetrahydroborate / methanol; dichloromethane / 3 h / 0 °C

4.1: dmap / dichloromethane / 0 - 20 °C

5.1: titanium tetrachloride / dichloromethane / 0.08 h / 0 °C

5.2: 1 h / 0 °C

6.1: water; sodium hydroxide / tetrahydrofuran; methanol; dichloromethane / 4 h / 20 °C

With dmap; sodium tetrahydroborate; n-butyllithium; water; titanium tetrachloride; acetic acid; diisopropylamine; sodium hydroxide; In tetrahydrofuran; methanol; hexane; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 1177423-25-4
3-(3-chloropyridin-4-yl)-3-oxopropanenitrile

: 1177423-30-1
C₂₃H₂₀N₂O₅

Guidance literature:: Multi-step reaction with 5 steps

1.1: acetic acid / N,N-dimethyl-formamide / 62 h / 140 °C

2.1: sodium tetrahydroborate / methanol; dichloromethane / 3 h / 0 °C

3.1: dmap / dichloromethane / 0 - 20 °C

4.1: titanium tetrachloride / dichloromethane / 0.08 h / 0 °C

4.2: 1 h / 0 °C

5.1: water; sodium hydroxide / tetrahydrofuran; methanol; dichloromethane / 4 h / 20 °C

With dmap; sodium tetrahydroborate; water; titanium tetrachloride; acetic acid; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;