1-(2,5-Dibenzyloxy-4-methylphenyl)-3-(dimethyl-amino)-propan-hydrochlorid

Base Information

Chemical Name:1-(2,5-Dibenzyloxy-4-methylphenyl)-3-(dimethyl-amino)-propan-hydrochlorid
CAS No.:91125-88-1
Molecular Formula:C₂₆H₃₁NO₂*ClH
Molecular Weight:425.999
Hs Code.:

Synonyms:1-(2,5-Dibenzyloxy-4-methylphenyl)-3-(dimethyl-amino)-propan-hydrochlorid

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Chemical Property of 1-(2,5-Dibenzyloxy-4-methylphenyl)-3-(dimethyl-amino)-propan-hydrochlorid

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Technology Process of 1-(2,5-Dibenzyloxy-4-methylphenyl)-3-(dimethyl-amino)-propan-hydrochlorid

There total 4 articles about 1-(2,5-Dibenzyloxy-4-methylphenyl)-3-(dimethyl-amino)-propan-hydrochlorid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 91125-85-8
1-(2,5-Dibenzyloxy-4-methyl-phenyl)-2-amino-propan

: 91125-88-1
1-(2,5-Dibenzyloxy-4-methylphenyl)-3-(dimethyl-amino)-propan-hydrochlorid

Guidance literature:: With formic acid; 1.) room temp., 3 h, 2.) 40 deg C, 6 h;
DOI:10.1002/ardp.19843170503

Reference yield:

: 40930-93-6
2,5-bis(benzyloxy)-4-methyl-benzaldehyde

: 91125-88-1
1-(2,5-Dibenzyloxy-4-methylphenyl)-3-(dimethyl-amino)-propan-hydrochlorid

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / ammonium acetate / 2 h / Heating

2: 80 percent / LiAlH₄ / tetrahydrofuran / 10 h / Heating

3: 60 percent / 1.) HCOOH / 1.) room temp., 3 h, 2.) 40 deg C, 6 h

With ammonium acetate; lithium aluminium tetrahydride; formic acid; In tetrahydrofuran;
DOI:10.1002/ardp.19843170503

Reference yield:

: 91126-02-2
1,4-bis-benzyloxy-2-methylbenzene

: 91125-88-1
1-(2,5-Dibenzyloxy-4-methylphenyl)-3-(dimethyl-amino)-propan-hydrochlorid

Guidance literature:: Multi-step reaction with 4 steps

1: 60 percent / POCl₃ / 3 h / 60 - 80 °C

2: 95 percent / ammonium acetate / 2 h / Heating

3: 80 percent / LiAlH₄ / tetrahydrofuran / 10 h / Heating

4: 60 percent / 1.) HCOOH / 1.) room temp., 3 h, 2.) 40 deg C, 6 h

With ammonium acetate; lithium aluminium tetrahydride; formic acid; trichlorophosphate; In tetrahydrofuran;
DOI:10.1002/ardp.19843170503