1-[({[5-(nitrooxy)hexyl]oxy}carbonyl)oxy]-1-methylethyl 2-ethoxy-1-{[2'-(1H-tetrazol-5-yl)biphenyl-4-yl]methyl}-1H-benzimidazole-7-carboxylate

Base Information

Chemical Name:1-[({[5-(nitrooxy)hexyl]oxy}carbonyl)oxy]-1-methylethyl 2-ethoxy-1-{[2'-(1H-tetrazol-5-yl)biphenyl-4-yl]methyl}-1H-benzimidazole-7-carboxylate
CAS No.:1186123-59-0
Molecular Formula:C₃₄H₃₇N₇O₉
Molecular Weight:687.709
Hs Code.:

Synonyms:1-[({[5-(nitrooxy)hexyl]oxy}carbonyl)oxy]-1-methylethyl 2-ethoxy-1-{[2'-(1H-tetrazol-5-yl)biphenyl-4-yl]methyl}-1H-benzimidazole-7-carboxylate

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Chemical Property of 1-[({[5-(nitrooxy)hexyl]oxy}carbonyl)oxy]-1-methylethyl 2-ethoxy-1-{[2'-(1H-tetrazol-5-yl)biphenyl-4-yl]methyl}-1H-benzimidazole-7-carboxylate

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Technology Process of 1-[({[5-(nitrooxy)hexyl]oxy}carbonyl)oxy]-1-methylethyl 2-ethoxy-1-{[2'-(1H-tetrazol-5-yl)biphenyl-4-yl]methyl}-1H-benzimidazole-7-carboxylate

There total 6 articles about 1-[({[5-(nitrooxy)hexyl]oxy}carbonyl)oxy]-1-methylethyl 2-ethoxy-1-{[2'-(1H-tetrazol-5-yl)biphenyl-4-yl]methyl}-1H-benzimidazole-7-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1186124-21-9
1-[({[5-(nitrooxy)hexyl]oxy}carbonyl)oxy]-1-methylethyl 2-ethoxy-1-{[2'-(1-trityl-1H-tetrazol-5-yl)biphenyl-4-yl]methyl}-1H-benzimidazole-7-carboxylate

: 1186123-59-0
1-[({[5-(nitrooxy)hexyl]oxy}carbonyl)oxy]-1-methylethyl 2-ethoxy-1-{[2'-(1H-tetrazol-5-yl)biphenyl-4-yl]methyl}-1H-benzimidazole-7-carboxylate

Guidance literature:: With methanol; at 90 ℃; for 0.333333h; Microwave irradiation;

Reference yield:

: 113493-16-6
C₁₃H₁₇NO₅

: 1186123-59-0
1-[({[5-(nitrooxy)hexyl]oxy}carbonyl)oxy]-1-methylethyl 2-ethoxy-1-{[2'-(1H-tetrazol-5-yl)biphenyl-4-yl]methyl}-1H-benzimidazole-7-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: 2,6-di-tert-butyl-4-methylpyridine; trifluoromethylsulfonic anhydride; tetraethylammonium nitrate / dichloromethane / -78 - 20 °C

2: water; sodium hydroxide / methanol / 3 h / 20 °C

3: dmap / dichloromethane / 12 h / 20 °C

4: methanol / 0.33 h / 90 °C / Microwave irradiation

With methanol; dmap; 2,6-di-tert-butyl-4-methylpyridine; trifluoromethylsulfonic anhydride; water; tetraethylammonium nitrate; sodium hydroxide; In methanol; dichloromethane;

Reference yield:

: 139481-72-4
2-Ethoxy-1-[[2'-(N-triphenylmethyltetrazol-5-yl)-biphenyl-4-yl]methyl]benzimidazole-7-carboxylic acid

: 1186123-59-0
1-[({[5-(nitrooxy)hexyl]oxy}carbonyl)oxy]-1-methylethyl 2-ethoxy-1-{[2'-(1H-tetrazol-5-yl)biphenyl-4-yl]methyl}-1H-benzimidazole-7-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: mercury(II) oxide / tetrahydrofuran / 24 h / 20 °C

1.2: 168 h / 20 °C

2.1: dmap / dichloromethane / 12 h / 20 °C

3.1: methanol / 0.33 h / 90 °C / Microwave irradiation

With methanol; dmap; mercury(II) oxide; In tetrahydrofuran; dichloromethane;