3-phenylperylene

Base Information

• Chemical Name: 3-phenylperylene
• CAS No.: 1256556-19-0
• Molecular Formula: C₂₆H₁₆
• Molecular Weight: 328.413
• Mol file: 1256556-19-0.mol

Synonyms:3-phenylperylene

Chemical Property of 3-phenylperylene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-phenylperylene

There total 4 articles about 3-phenylperylene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

3-bromoperylene (23683-68-3) + phenylboronic acid (98-80-6) → 3-phenylperylene (1256556-19-0)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In ethanol; water; toluene; for 8h; Inert atmosphere; Reflux;

DOI:10.1021/jo402718e

Reference yield: 18.0%

4,4,5,5-tetramethyl-2-((perylene-3-yl)phenyl)-1,3,2-dioxaborolan (950761-81-6) + bromobenzene (108-86-1,52753-63-6) → 3-phenylperylene (1256556-19-0)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In tetrahydrofuran; water; at 100 ℃; for 3h; Inert atmosphere; Microwave irradiation;

DOI:10.1002/anie.201911025

Reference yield: 17.0%

triphenylboroxine (3262-89-3) + PERYLENE (198-55-0) → 3,4,9-triphenylperylene (1415803-83-6) + 3-phenylperylene (1256556-19-0) + 3,4,9,10-tetraphenylperylene

Guidance literature:

With o-tetrachloroquinone; palladium diacetate; In 1,2-dichloro-ethane; at 80 ℃; for 2h; Inert atmosphere;

DOI:10.1016/j.tet.2013.01.037

upstream raw materials:

triphenylboroxine

PERYLENE

3-bromoperylene

phenylboronic acid