1-tert-butoxycarbonyl-1-(3,5-di-tert-butylphenyl)hydrazine

Base Information

• Chemical Name: 1-tert-butoxycarbonyl-1-(3,5-di-tert-butylphenyl)hydrazine
• CAS No.: 1032697-06-5
• Molecular Formula: C₁₉H₃₂N₂O₂
• Molecular Weight: 320.475
• Mol file: 1032697-06-5.mol

Synonyms:1-tert-butoxycarbonyl-1-(3,5-di-tert-butylphenyl)hydrazine

Chemical Property of 1-tert-butoxycarbonyl-1-(3,5-di-tert-butylphenyl)hydrazine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-tert-butoxycarbonyl-1-(3,5-di-tert-butylphenyl)hydrazine

There total 1 articles about 1-tert-butoxycarbonyl-1-(3,5-di-tert-butylphenyl)hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

t-butoxycarbonylhydrazine (870-46-2) + 1,3-di(tert-butyl)-5-iodobenzene (37055-53-1) → 1-tert-butoxycarbonyl-1-(3,5-di-tert-butylphenyl)hydrazine (1032697-06-5)

Guidance literature:

With copper(l) iodide; 1,10-Phenanthroline; caesium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 23h; Inert atmosphere;

DOI:10.1002/anie.200802050

Reference yield: 55.0%

C13H14BrNO2 (1032697-08-7) + 1-tert-butoxycarbonyl-1-(3,5-di-tert-butylphenyl)hydrazine (1032697-06-5) → C32H45N3O4 (1032697-10-1)

Guidance literature:

With tri-tert-butyl phosphine; palladium diacetate; caesium carbonate; In toluene; at 20 - 120 ℃; for 2.5h; Inert atmosphere; Sealed tube;

DOI:10.1002/anie.200802050

Reference yield: 54.0%

1-tert-butoxycarbonyl-1-(3,5-di-tert-butylphenyl)hydrazine (1032697-06-5) + C16H20BrNO2 (1055421-92-5) → C35H51N3O4 (1055421-98-1)

Guidance literature:

With tri-tert-butyl phosphine; palladium diacetate; caesium carbonate; In toluene; at 120 ℃; for 3h; Inert atmosphere; Sealed tube;

DOI:10.1002/anie.200802050

upstream raw materials:

t-butoxycarbonylhydrazine

1,3-di(tert-butyl)-5-iodobenzene

Downstream raw materials:

C₃₂H₄₅N₃O₄

C₃₅H₅₁N₃O₄