1-cyano-1-(4-(trifluoromethyl)phenyl)ethyl diethyl phosphate

Base Information

• Chemical Name: 1-cyano-1-(4-(trifluoromethyl)phenyl)ethyl diethyl phosphate
• CAS No.: 1469462-84-7
• Molecular Formula: C₁₄H₁₇F₃NO₄P
• Molecular Weight: 351.262
• Mol file: 1469462-84-7.mol

Synonyms:1-cyano-1-(4-(trifluoromethyl)phenyl)ethyl diethyl phosphate

Chemical Property of 1-cyano-1-(4-(trifluoromethyl)phenyl)ethyl diethyl phosphate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 1-cyano-1-(4-(trifluoromethyl)phenyl)ethyl diethyl phosphate

There total 1 articles about 1-cyano-1-(4-(trifluoromethyl)phenyl)ethyl diethyl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

diethyl cyanophosphonate (2942-58-7) + 1-(4-trifluoromethylphenyl)ethanone (709-63-7) → 1-cyano-1-(4-(trifluoromethyl)phenyl)ethyl diethyl phosphate (1469462-84-7)

Guidance literature:

With 1,3-bis-(2,6-diisopropylphenyl)-imidazol-2-ylidene; In toluene; at 20 ℃; for 2h; Inert atmosphere;

DOI:10.1016/j.tetlet.2013.08.073

Reference yield: 85.0%

1-cyano-1-(4-(trifluoromethyl)phenyl)ethyl diethyl phosphate (1469462-84-7) → 1-(prop-1-ynyl)-4-trifluoromethylbenzene (79756-87-9)

Guidance literature:

With trimethylsilylazide;

DOI:10.1021/acs.joc.7b00346

upstream raw materials:

diethyl cyanophosphonate

1-(4-trifluoromethylphenyl)ethanone

Downstream raw materials:

1-(prop-1-ynyl)-4-trifluoromethylbenzene