5,5’-(naphthalene-2,7-diyl)di(isophthalic acid)

Base Information

Chemical Name:5,5’-(naphthalene-2,7-diyl)di(isophthalic acid)
CAS No.:1426343-45-4
Molecular Formula:C₂₆H₁₆O₈
Molecular Weight:456.408
Hs Code.:

Synonyms:5,5’-(naphthalene-2,7-diyl)di(isophthalic acid)

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Chemical Property of 5,5’-(naphthalene-2,7-diyl)di(isophthalic acid)

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Technology Process of 5,5’-(naphthalene-2,7-diyl)di(isophthalic acid)

There total 3 articles about 5,5’-(naphthalene-2,7-diyl)di(isophthalic acid) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: tetramethyl 5,5’-(naphthalene-2,7-diyl)di(isophthalate)

: 1426343-45-4
5,5’-(naphthalene-2,7-diyl)di(isophthalic acid)

Guidance literature:: With water; sodium hydroxide; In tetrahydrofuran; methanol; Reflux;
DOI:10.1039/c7dt04087c

Reference yield: 91.0%

: 1426343-46-5
tetraethyl 5,5'-(naphthalene-2,7-diyl)diisophthalate

: 1426343-45-4
5,5’-(naphthalene-2,7-diyl)di(isophthalic acid)

Guidance literature:: With water; sodium hydroxide; In tetrahydrofuran; methanol; at 20 ℃;

Reference yield:

: 58556-75-5
2,7-dibromonaphthalene

: 1309982-02-2
diethyl 5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1,3-benzene-dicarboxylate

: 1426343-45-4
5,5’-(naphthalene-2,7-diyl)di(isophthalic acid)

Guidance literature:: Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; cesium fluoride / 1,2-dimethoxyethane / 48 h / Inert atmosphere; Reflux; Schlenk technique

2: water; sodium hydroxide / tetrahydrofuran; methanol / 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; water; cesium fluoride; sodium hydroxide; In tetrahydrofuran; methanol; 1,2-dimethoxyethane;