1,3-dinonyl-1-((1S,2S,3R,4R,5S,6R)-2,3,4,5-tetrakis(benzyloxy)-6-hydroxycyclohexyl)thiourea

Base Information

Chemical Name:1,3-dinonyl-1-((1S,2S,3R,4R,5S,6R)-2,3,4,5-tetrakis(benzyloxy)-6-hydroxycyclohexyl)thiourea
CAS No.:1287225-83-5
Molecular Formula:C₅₃H₇₄N₂O₅S
Molecular Weight:851.247
Hs Code.:

Synonyms:1,3-dinonyl-1-((1S,2S,3R,4R,5S,6R)-2,3,4,5-tetrakis(benzyloxy)-6-hydroxycyclohexyl)thiourea

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Chemical Property of 1,3-dinonyl-1-((1S,2S,3R,4R,5S,6R)-2,3,4,5-tetrakis(benzyloxy)-6-hydroxycyclohexyl)thiourea

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Technology Process of 1,3-dinonyl-1-((1S,2S,3R,4R,5S,6R)-2,3,4,5-tetrakis(benzyloxy)-6-hydroxycyclohexyl)thiourea

There total 7 articles about 1,3-dinonyl-1-((1S,2S,3R,4R,5S,6R)-2,3,4,5-tetrakis(benzyloxy)-6-hydroxycyclohexyl)thiourea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 4430-43-7
n-nonyl isothiocyanate

: 1287225-52-8
(1R,2S,3R,4R,5S,6S)-2,3,4,5-tetrakis(benzyloxy)-6-(nonylamino)cyclohexanol

: 1287225-83-5
1,3-dinonyl-1-((1S,2S,3R,4R,5S,6R)-2,3,4,5-tetrakis(benzyloxy)-6-hydroxycyclohexyl)thiourea

Guidance literature:: In tetrahydrofuran; at 45 ℃; for 18h; chemoselective reaction;
DOI:10.1021/ja111480z

Reference yield:

: 124-19-6
nonan-1-al

: 1287225-83-5
1,3-dinonyl-1-((1S,2S,3R,4R,5S,6R)-2,3,4,5-tetrakis(benzyloxy)-6-hydroxycyclohexyl)thiourea

Guidance literature:: Multi-step reaction with 2 steps

1: sodium cyanoborohydride; acetic acid / methanol / 4 h / 20 °C / Inert atmosphere

2: tetrahydrofuran / 18 h / 45 °C

With sodium cyanoborohydride; acetic acid; In tetrahydrofuran; methanol;
DOI:10.1021/ja111480z

Reference yield:

: 1287225-40-4
(1S,2S,3R,4R,5S,6S)-N-(2,3,4,5-tetrakis(benzyloxy)-6-hydroxycyclohexyl)carbamic acid tert-butyl ester

: 1287225-83-5
1,3-dinonyl-1-((1S,2S,3R,4R,5S,6R)-2,3,4,5-tetrakis(benzyloxy)-6-hydroxycyclohexyl)thiourea

Guidance literature:: Multi-step reaction with 5 steps

1: triethylamine / tetrahydrofuran / 5 h / 0 - 20 °C

2: N,N-dimethyl-formamide / 16 h / 110 °C

3: ethanol; sodium hydroxide / 16 h / 80 °C

4: sodium cyanoborohydride; acetic acid / methanol / 4 h / 20 °C / Inert atmosphere

5: tetrahydrofuran / 18 h / 45 °C

With ethanol; sodium cyanoborohydride; acetic acid; triethylamine; sodium hydroxide; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1021/ja111480z