7-amino-2-(4-tert-butoxybenzyl)-4-[2-(4-methoxyphenyl)-ethyl]-1,2,4,5-tetrahydro-3H-1,4-benzodiazepin-3-one

Base Information

Chemical Name:7-amino-2-(4-tert-butoxybenzyl)-4-[2-(4-methoxyphenyl)-ethyl]-1,2,4,5-tetrahydro-3H-1,4-benzodiazepin-3-one
CAS No.:1168016-28-1
Molecular Formula:C₂₉H₃₅N₃O₃
Molecular Weight:473.615
Hs Code.:

Synonyms:7-amino-2-(4-tert-butoxybenzyl)-4-[2-(4-methoxyphenyl)-ethyl]-1,2,4,5-tetrahydro-3H-1,4-benzodiazepin-3-one

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Chemical Property of 7-amino-2-(4-tert-butoxybenzyl)-4-[2-(4-methoxyphenyl)-ethyl]-1,2,4,5-tetrahydro-3H-1,4-benzodiazepin-3-one

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Technology Process of 7-amino-2-(4-tert-butoxybenzyl)-4-[2-(4-methoxyphenyl)-ethyl]-1,2,4,5-tetrahydro-3H-1,4-benzodiazepin-3-one

There total 1 articles about 7-amino-2-(4-tert-butoxybenzyl)-4-[2-(4-methoxyphenyl)-ethyl]-1,2,4,5-tetrahydro-3H-1,4-benzodiazepin-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1168015-94-8
2-(4-tert-butoxybenzyl)-4-[2-(4-methoxyphenyl)ethyl]-7-nitro-1,2,4,5-tetrahydro-3H-1,4-benzodiazepin-3-one

: 1168016-28-1
7-amino-2-(4-tert-butoxybenzyl)-4-[2-(4-methoxyphenyl)-ethyl]-1,2,4,5-tetrahydro-3H-1,4-benzodiazepin-3-one

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; for 3h; under 30402 Torr;
DOI:10.1016/j.tet.2009.03.095

Reference yield: 68.0%

: 1168016-28-1
7-amino-2-(4-tert-butoxybenzyl)-4-[2-(4-methoxyphenyl)-ethyl]-1,2,4,5-tetrahydro-3H-1,4-benzodiazepin-3-one

: 71989-14-5
Fmoc-(tBu)Asp-OH

: 1168016-32-7
C₅₂H₅₈N₄O₈

Guidance literature:: With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2009.03.095

Reference yield: 46.0%

: 1168016-28-1
7-amino-2-(4-tert-butoxybenzyl)-4-[2-(4-methoxyphenyl)-ethyl]-1,2,4,5-tetrahydro-3H-1,4-benzodiazepin-3-one

: 71989-38-3,118488-18-9,204384-67-8
Fmoc-Tyr(tBu)-OH

: 1168016-35-0
C₅₇H₆₂N₄O₇

Guidance literature:: With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2009.03.095