methyl (6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->2)-6,7-di-O-acetyl-L-glycero-α-D-manno-heptopyranoside

Base Information

Chemical Name:methyl (6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->2)-6,7-di-O-acetyl-L-glycero-α-D-manno-heptopyranoside
CAS No.:688044-81-7
Molecular Formula:C₃₄H₄₃N₃O₁₄
Molecular Weight:717.727
Hs Code.:

Synonyms:methyl (6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->2)-6,7-di-O-acetyl-L-glycero-α-D-manno-heptopyranoside

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Chemical Property of methyl (6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->2)-6,7-di-O-acetyl-L-glycero-α-D-manno-heptopyranoside

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Technology Process of methyl (6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->2)-6,7-di-O-acetyl-L-glycero-α-D-manno-heptopyranoside

There total 1 articles about methyl (6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->2)-6,7-di-O-acetyl-L-glycero-α-D-manno-heptopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: (2'S,3'S)-methyl (6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->2)-6,7-di-O-acetyl-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-L-glycero-α-D-manno-heptopyranoside

: 688044-81-7
methyl (6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->2)-6,7-di-O-acetyl-L-glycero-α-D-manno-heptopyranoside

Guidance literature:: With water; trifluoroacetic acid; at 20 ℃; for 0.25h;
DOI:10.1002/ejoc.200300652

Reference yield: 88.0%

: 994-30-9
triethylsilyl chloride

: 108-24-7
acetic anhydride

: 688044-81-7
methyl (6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->2)-6,7-di-O-acetyl-L-glycero-α-D-manno-heptopyranoside

: methyl (6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->2)-4,6,7-tri-O-acetyl-3-O-triethylsilyl-L-glycero-α-D-manno-heptopyranoside

Guidance literature:: triethylsilyl chloride; methyl (6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->2)-6,7-di-O-acetyl-L-glycero-α-D-manno-heptopyranoside; In pyridine; at 0 - 20 ℃; for 1h;

acetic anhydride; In pyridine; at 20 ℃; for 72h; Further stages.;
DOI:10.1002/ejoc.200300652