Technology Process of C58H93N15O4S
There total 17 articles about C58H93N15O4S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triethylsilane; trifluoroacetic acid;
In
dichloromethane;
at 20 - 26 ℃;
for 18h;
Inert atmosphere;
DOI:10.1039/c1nj20206e
- Guidance literature:
-
With
triethylsilane; trifluoroacetic acid;
In
dichloromethane;
at 20 - 26 ℃;
Inert atmosphere;
DOI:10.1016/j.tet.2013.01.070
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: sodium hydroxide / tetrahydrofuran; water / 0 °C
1.2: 2 h / 0 °C
2.1: thiourea / ethanol / 24 h / Reflux; Inert atmosphere
2.2: 3 h / Reflux; Inert atmosphere
3.1: trifluoroacetic acid / dichloromethane / 0.25 h / 20 - 26 °C / Inert atmosphere
3.2: 5 h / 20 - 26 °C / Inert atmosphere
4.1: sodium hydroxide / tetrahydrofuran; water / 20 - 26 °C
4.2: 24 h / 20 - 26 °C / Inert atmosphere
5.1: lithium bromide / acetone / 24 h / Reflux
6.1: sodium hydride / tetrahydrofuran; mineral oil / 3 h / Inert atmosphere
6.2: 72 h / 20 - 26 °C / Inert atmosphere
7.1: triethylsilane; trifluoroacetic acid / dichloromethane / 18 h / 20 - 26 °C / Inert atmosphere
With
triethylsilane; sodium hydride; thiourea; trifluoroacetic acid; lithium bromide; sodium hydroxide;
In
tetrahydrofuran; ethanol; dichloromethane; water; acetone; mineral oil;
DOI:10.1039/c1nj20206e