2-(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-2-(2,4,6-triisopropylphenyl)-4-(phenylimino)-1,3,2-dithiastannetane

Base Information

Chemical Name:2-(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-2-(2,4,6-triisopropylphenyl)-4-(phenylimino)-1,3,2-dithiastannetane
CAS No.:147424-56-4
Molecular Formula:C₄₉H₈₇NS₂Si₆Sn
Molecular Weight:1041.59
Hs Code.:

Synonyms:2-(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-2-(2,4,6-triisopropylphenyl)-4-(phenylimino)-1,3,2-dithiastannetane

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Chemical Property of 2-(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-2-(2,4,6-triisopropylphenyl)-4-(phenylimino)-1,3,2-dithiastannetane

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Technology Process of 2-(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-2-(2,4,6-triisopropylphenyl)-4-(phenylimino)-1,3,2-dithiastannetane

There total 4 articles about 2-(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-2-(2,4,6-triisopropylphenyl)-4-(phenylimino)-1,3,2-dithiastannetane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 147451-69-2
(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)(2,4,6-triisopropylphenyl)SnS

: 103-72-0
phenyl isothiocyanate

: 147424-56-4
2-(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-2-(2,4,6-triisopropylphenyl)-4-(phenylimino)-1,3,2-dithiastannetane

Guidance literature:: In hexane;

Reference yield: 38.0%

: 1498-99-3
styrenesulfide

: 21524-34-5
2,4,6-triisopropyl-1-bromobenzene

: 115160-05-9
1-bromo-2,4,6-tris[bis(trimethylsilyl)methyl]benzene

: 103-72-0
phenyl isothiocyanate

: tin(ll) chloride

: 147424-56-4
2-(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-2-(2,4,6-triisopropylphenyl)-4-(phenylimino)-1,3,2-dithiastannetane

Guidance literature:: With t-BuLi; In tetrahydrofuran; diethyl ether; Ar-atmosphere; stirring (-45°C, 1 h), PhNCS addn. (room temp.); evapn., chromy. (SiO2); elem .anal.;
DOI:10.1021/om960449u

Reference yield: 22.0%

: 7782-49-2
selenium

: 21524-34-5
2,4,6-triisopropyl-1-bromobenzene

: 115160-05-9
1-bromo-2,4,6-tris[bis(trimethylsilyl)methyl]benzene

: 103-72-0
phenyl isothiocyanate

: tin(ll) chloride

: 147424-56-4
2-(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-2-(2,4,6-triisopropylphenyl)-4-(phenylimino)-1,3,2-dithiastannetane

: 170703-57-8
2-tris[bis(trimethylsilyl)methyl]phenyl-2-(2,4,6-triisopropylphenyl)-4-phenylimino-1,3,2-diselenastannetane

Guidance literature:: With tert.-butyl lithium; In tetrahydrofuran; diethyl ether; pentane; Ar-atmosphere; treatment of SnCl2 (in ether) with Li-salts of ligands (from bromides in THF and t-BuLi in pentane), addn. of 1 equiv. Se, stirring at -70°C for 2.5 h, addn. of PhNCS, warming to room temp.; solvent removal, chromy. (SiO2); elem. anal.;
DOI:10.1016/0022-328X(95)00334-M