2-amino-3-phenyl-1,2,3,4-tetrahydroisoquinoline hydrochloride

Base Information

Chemical Name:2-amino-3-phenyl-1,2,3,4-tetrahydroisoquinoline hydrochloride
CAS No.:85741-17-9
Molecular Formula:C₁₅H₁₆N₂*ClH
Molecular Weight:260.766
Hs Code.:

Synonyms:2-amino-3-phenyl-1,2,3,4-tetrahydroisoquinoline hydrochloride

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Chemical Property of 2-amino-3-phenyl-1,2,3,4-tetrahydroisoquinoline hydrochloride

Chemical Property:

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Technology Process of 2-amino-3-phenyl-1,2,3,4-tetrahydroisoquinoline hydrochloride

There total 6 articles about 2-amino-3-phenyl-1,2,3,4-tetrahydroisoquinoline hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 85741-16-8
2-Nitroso-3-phenyl-1,2,3,4-tetrahydroisoquinoline

: 85741-17-9
2-amino-3-phenyl-1,2,3,4-tetrahydroisoquinoline hydrochloride

Guidance literature:: With hydrogenchloride; sodium hydroxide; sodium disulfite; In ethanol; at 50 ℃; for 5h;

Reference yield:

: 7115-13-1
3-phenyl-2H-isoquinolin-1-one

: 85741-17-9
2-amino-3-phenyl-1,2,3,4-tetrahydroisoquinoline hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: 84 percent / POCl₃ / 0.5 h / Heating

2: 32.7 g / amalgamated zinc dust, conc. HCl / ethanol / 72 h / Heating

3: 77 percent / sodium nitrite, acetic acid / H₂O / 2 h / 75 °C

4: 56 percent / 1.) 20percent aq.NaOH, sodium hydrosulfite, 2.) 10N HCl / ethanol / 5 h / 50 °C

With hydrogenchloride; sodium hydroxide; sodium disulfite; amalgamated zinc; acetic acid; sodium nitrite; trichlorophosphate; In ethanol; water;

Reference yield:

: 78318-00-0
3-phenyl-1,2,3,4-tetrahydroisoquinoline

: 85741-17-9
2-amino-3-phenyl-1,2,3,4-tetrahydroisoquinoline hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / sodium nitrite, acetic acid / H₂O / 2 h / 75 °C

2: 56 percent / 1.) 20percent aq.NaOH, sodium hydrosulfite, 2.) 10N HCl / ethanol / 5 h / 50 °C

With hydrogenchloride; sodium hydroxide; sodium disulfite; acetic acid; sodium nitrite; In ethanol; water;