2-allyl-1-[(2-allyl-3-isopropoxy-4-methoxybenzyl)oxy]-3-isopropoxy-4-methoxybenzene

Base Information

Chemical Name:2-allyl-1-[(2-allyl-3-isopropoxy-4-methoxybenzyl)oxy]-3-isopropoxy-4-methoxybenzene
CAS No.:881199-45-7
Molecular Formula:C₂₇H₃₆O₅
Molecular Weight:440.58
Hs Code.:

Synonyms:2-allyl-1-[(2-allyl-3-isopropoxy-4-methoxybenzyl)oxy]-3-isopropoxy-4-methoxybenzene

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Chemical Property of 2-allyl-1-[(2-allyl-3-isopropoxy-4-methoxybenzyl)oxy]-3-isopropoxy-4-methoxybenzene

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Technology Process of 2-allyl-1-[(2-allyl-3-isopropoxy-4-methoxybenzyl)oxy]-3-isopropoxy-4-methoxybenzene

There total 5 articles about 2-allyl-1-[(2-allyl-3-isopropoxy-4-methoxybenzyl)oxy]-3-isopropoxy-4-methoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 634616-23-2
(2-allyl-3-isopropoxy-4-methoxyphenyl)methanol

: 767290-03-9
2-allyl-3-isopropoxy-4-methoxyphenol

: 881199-45-7
2-allyl-1-[(2-allyl-3-isopropoxy-4-methoxybenzyl)oxy]-3-isopropoxy-4-methoxybenzene

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 12h;
DOI:10.3987/COM-05-10592

Reference yield:

: 621-59-0
isovanillin

: 881199-45-7
2-allyl-1-[(2-allyl-3-isopropoxy-4-methoxybenzyl)oxy]-3-isopropoxy-4-methoxybenzene

Guidance literature:: Multi-step reaction with 5 steps

1: 87 percent / K₂CO₃ / acetone / 8 h / Heating

2: 92 percent / 3 h / 180 °C

3: K₂CO₃ / acetone / 8 h / Heating

4: H₂O₂; H⁽¹⁺⁾ / methanol / 1.5 h / 20 °C

5: 58 percent / triphenylphosphane; diisopropyl diazenedicarboxylate / tetrahydrofuran / 12 h / 20 °C

With di-isopropyl azodicarboxylate; dihydrogen peroxide; hydrogen cation; potassium carbonate; triphenylphosphine; In tetrahydrofuran; methanol; acetone; 2: Claisen rearrangement / 4: Dakin oxidation / 5: Mitsunobu reaction;
DOI:10.3987/COM-05-10592

Reference yield:

: 18075-40-6
O-allylisovanillin

: 881199-45-7
2-allyl-1-[(2-allyl-3-isopropoxy-4-methoxybenzyl)oxy]-3-isopropoxy-4-methoxybenzene

Guidance literature:: Multi-step reaction with 4 steps

1: 92 percent / 3 h / 180 °C

2: K₂CO₃ / acetone / 8 h / Heating

3: H₂O₂; H⁽¹⁺⁾ / methanol / 1.5 h / 20 °C

4: 58 percent / triphenylphosphane; diisopropyl diazenedicarboxylate / tetrahydrofuran / 12 h / 20 °C

With di-isopropyl azodicarboxylate; dihydrogen peroxide; hydrogen cation; potassium carbonate; triphenylphosphine; In tetrahydrofuran; methanol; acetone; 1: Claisen rearrangement / 3: Dakin oxidation / 4: Mitsunobu reaction;
DOI:10.3987/COM-05-10592