(S)-5-[(2,4-Dimethoxy-3-methyl-phenyl)-dimethoxy-methyl]-dihydro-furan-2-one

Base Information

Chemical Name:(S)-5-[(2,4-Dimethoxy-3-methyl-phenyl)-dimethoxy-methyl]-dihydro-furan-2-one
CAS No.:627077-40-1
Molecular Formula:C₁₆H₂₂O₆
Molecular Weight:310.347
Hs Code.:

Synonyms:(S)-5-[(2,4-Dimethoxy-3-methyl-phenyl)-dimethoxy-methyl]-dihydro-furan-2-one

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Chemical Property of (S)-5-[(2,4-Dimethoxy-3-methyl-phenyl)-dimethoxy-methyl]-dihydro-furan-2-one

Chemical Property:

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Technology Process of (S)-5-[(2,4-Dimethoxy-3-methyl-phenyl)-dimethoxy-methyl]-dihydro-furan-2-one

There total 3 articles about (S)-5-[(2,4-Dimethoxy-3-methyl-phenyl)-dimethoxy-methyl]-dihydro-furan-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 627077-50-3
(S)-5-(2,4-Dimethoxy-3-methyl-benzoyl)-dihydro-furan-2-one

: 149-73-5
trimethyl orthoformate

: 627077-40-1
(S)-5-[(2,4-Dimethoxy-3-methyl-phenyl)-dimethoxy-methyl]-dihydro-furan-2-one

Guidance literature:: (S)-5-(2,4-Dimethoxy-3-methyl-benzoyl)-dihydro-furan-2-one; trimethyl orthoformate; With toluene-4-sulfonic acid; In methanol;

With potassium tert-butylate; In tetrahydrofuran; methanol;
DOI:10.1021/ja035898h

Reference yield:

: 54848-33-8
(S)-tetrahydro-5-oxo-2-furancarbonyl chloride

: 627077-40-1
(S)-5-[(2,4-Dimethoxy-3-methyl-phenyl)-dimethoxy-methyl]-dihydro-furan-2-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: 75 percent / ZnCl₂; PdCl₂(PPh₃)2 / tetrahydrofuran

2.1: TsOH / methanol

2.2: 83 percent / t-BuOK / tetrahydrofuran; methanol

With bis-triphenylphosphine-palladium(II) chloride; toluene-4-sulfonic acid; zinc(II) chloride; In tetrahydrofuran; methanol;
DOI:10.1021/ja035898h

Reference yield:

: C₉H₁₁BrMgO₂

: 627077-40-1
(S)-5-[(2,4-Dimethoxy-3-methyl-phenyl)-dimethoxy-methyl]-dihydro-furan-2-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: 75 percent / ZnCl₂; PdCl₂(PPh₃)2 / tetrahydrofuran

2.1: TsOH / methanol

2.2: 83 percent / t-BuOK / tetrahydrofuran; methanol

With bis-triphenylphosphine-palladium(II) chloride; toluene-4-sulfonic acid; zinc(II) chloride; In tetrahydrofuran; methanol;
DOI:10.1021/ja035898h