Technology Process of C27H29NO5
There total 9 articles about C27H29NO5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
In
chloroform;
at 50 ℃;
for 0.666667h;
stereospecific reaction;
UV-irradiation;
Inert atmosphere;
DOI:10.1016/j.tetasy.2011.06.007
- Guidance literature:
-
Multi-step reaction with 5 steps
1: lithium hydroxide / ethanol / Reflux
2: acetyl chloride / 8 h / Reflux
3: triethylamine / dichloromethane
4: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine / tetrahydrofuran / 35 °C / Cooling with ice
5: chloroform / 0.67 h / 50 °C / UV-irradiation; Inert atmosphere
With
(benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; acetyl chloride; lithium hydroxide;
In
tetrahydrofuran; ethanol; dichloromethane; chloroform;
DOI:10.1016/j.tetasy.2011.06.007
- Guidance literature:
-
Multi-step reaction with 6 steps
1: potassium carbonate / dimethyl sulfoxide; acetone / 15 h / Reflux
2: lithium hydroxide / ethanol / Reflux
3: acetyl chloride / 8 h / Reflux
4: triethylamine / dichloromethane
5: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine / tetrahydrofuran / 35 °C / Cooling with ice
6: chloroform / 0.67 h / 50 °C / UV-irradiation; Inert atmosphere
With
potassium carbonate; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; acetyl chloride; lithium hydroxide;
In
tetrahydrofuran; ethanol; dichloromethane; chloroform; dimethyl sulfoxide; acetone;
DOI:10.1016/j.tetasy.2011.06.007
