4-ethyl-4-methoxy-cyclohexanol

Base Information

Chemical Name:4-ethyl-4-methoxy-cyclohexanol
CAS No.:906318-29-4
Molecular Formula:C₉H₁₈O₂
Molecular Weight:158.241
Hs Code.:

Synonyms:4-ethyl-4-methoxy-cyclohexanol

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Chemical Property of 4-ethyl-4-methoxy-cyclohexanol

Chemical Property:

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Technology Process of 4-ethyl-4-methoxy-cyclohexanol

There total 4 articles about 4-ethyl-4-methoxy-cyclohexanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 557-20-0
diethylzinc

: 220061-72-3
(4,4-dimethoxy-cyclohexyloxymethyl)-benzene

: 906318-29-4
4-ethyl-4-methoxy-cyclohexanol

Guidance literature:: diethylzinc; (4,4-dimethoxy-cyclohexyloxymethyl)-benzene; With trimethylsilyl trifluoromethanesulfonate; In hexane; dichloromethane; at -78 - 0 ℃;

With hydrogen; palladium on activated charcoal; In ethanol; for 24h; under 760 Torr;
DOI:10.1021/jo060968z

Reference yield:

: 2987-06-6
4-(benzyloxy)cyclohexanone

: 906318-29-4
4-ethyl-4-methoxy-cyclohexanol

Guidance literature:: Multi-step reaction with 2 steps

1.1: 91 percent / p-toluenesulfonic acid / methanol / 24 h

2.1: Me₃SiOTf / CH₂Cl₂; hexane / -78 - 0 °C

2.2: 0.06 g / H₂ / Pd/C / ethanol / 24 h / 760 Torr

With trimethylsilyl trifluoromethanesulfonate; toluene-4-sulfonic acid; In methanol; hexane; dichloromethane;
DOI:10.1021/jo060968z

Reference yield:

: 2976-80-9
4-(benzyloxy)cyclohexan-1-ol

: 906318-29-4
4-ethyl-4-methoxy-cyclohexanol

Guidance literature:: Multi-step reaction with 3 steps

1.1: 99 percent / oxalyl chloride; DMSO; Et₃N / CH₂Cl₂ / -40 - 0 °C

2.1: 91 percent / p-toluenesulfonic acid / methanol / 24 h

3.1: Me₃SiOTf / CH₂Cl₂; hexane / -78 - 0 °C

3.2: 0.06 g / H₂ / Pd/C / ethanol / 24 h / 760 Torr

With oxalyl dichloride; trimethylsilyl trifluoromethanesulfonate; toluene-4-sulfonic acid; dimethyl sulfoxide; triethylamine; In methanol; hexane; dichloromethane; 1.1: Swern oxidation;
DOI:10.1021/jo060968z