7-Oxabicyclo[4.1.0]heptane, 1-(1,3-dimethyl-1,3-butadienyl}-2,2,6-trimethyl- (E)-

Base Information

Chemical Name:7-Oxabicyclo[4.1.0]heptane, 1-(1,3-dimethyl-1,3-butadienyl}-2,2,6-trimethyl- (E)-
CAS No.:89128-14-3
Molecular Formula:C₁₅H₂₄O
Molecular Weight:220.355
Hs Code.:

Synonyms:7-Oxabicyclo[4.1.0]heptane, 1-(1,3-dimethyl-1,3-butadienyl}-2,2,6-trimethyl- (E)-

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Chemical Property of 7-Oxabicyclo[4.1.0]heptane, 1-(1,3-dimethyl-1,3-butadienyl}-2,2,6-trimethyl- (E)-

Chemical Property:

Boiling Point:267.1±9.0 °C(Predicted)
PSA：12.53000
Density:0.947±0.06 g/cm3(Predicted)
LogP:4.24660

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

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Technology Process of 7-Oxabicyclo[4.1.0]heptane, 1-(1,3-dimethyl-1,3-butadienyl}-2,2,6-trimethyl- (E)-

There total 5 articles about 7-Oxabicyclo[4.1.0]heptane, 1-(1,3-dimethyl-1,3-butadienyl}-2,2,6-trimethyl- (E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 89128-12-1,89128-13-2
(E)-4-(2',6',6'-trimethyl-1',2'-epoxycyclohexyl)-3-penten-2-one

: 19493-09-5
Methylenetriphenylphosphorane

: 89128-14-3,89128-15-4
1-[(1E)-1,3-Dimethyl-1,3-butadienyl]-2,2,6-trimethyl-7-oxabicyclo[4.1.0]heptane

Guidance literature:: In diethyl ether;
DOI:10.1016/S0040-4020(01)88624-5

Reference yield: 60.0%

: 89128-12-1,89128-13-2
(Z)-4-((1R,6R)-2,2,6-Trimethyl-7-oxa-bicyclo[4.1.0]hept-1-yl)-pent-3-en-2-one

: 19493-09-5
Methylenetriphenylphosphorane

: 89128-14-3,89128-15-4
(1R,6R)-1-((Z)-1,3-Dimethyl-buta-1,3-dienyl)-2,2,6-trimethyl-7-oxa-bicyclo[4.1.0]heptane

Guidance literature:: In diethyl ether;
DOI:10.1016/S0040-4020(01)88624-5

Reference yield:

: 79892-19-6
(Z)-4-(2',6',6'-trimethyl-1'-cyclohexen-1'yl)-3-penten-2-one

: 89128-14-3,89128-15-4
(1R,6R)-1-((Z)-1,3-Dimethyl-buta-1,3-dienyl)-2,2,6-trimethyl-7-oxa-bicyclo[4.1.0]heptane

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / m-CPBA / diethyl ether

2: 60 percent / diethyl ether

With 3-chloro-benzenecarboperoxoic acid; In diethyl ether;
DOI:10.1016/S0040-4020(01)88624-5