ethyl 3-{2-[(triphenylmethylsulfanyl)methylcarbonylamino]ethanamido}-4-hydroxybenzoate

Base Information

Chemical Name:ethyl 3-{2-[(triphenylmethylsulfanyl)methylcarbonylamino]ethanamido}-4-hydroxybenzoate
CAS No.:886983-43-3
Molecular Formula:C₃₂H₃₀N₂O₅S
Molecular Weight:554.667
Hs Code.:

Synonyms:ethyl 3-{2-[(triphenylmethylsulfanyl)methylcarbonylamino]ethanamido}-4-hydroxybenzoate

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Chemical Property of ethyl 3-{2-[(triphenylmethylsulfanyl)methylcarbonylamino]ethanamido}-4-hydroxybenzoate

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Technology Process of ethyl 3-{2-[(triphenylmethylsulfanyl)methylcarbonylamino]ethanamido}-4-hydroxybenzoate

There total 3 articles about ethyl 3-{2-[(triphenylmethylsulfanyl)methylcarbonylamino]ethanamido}-4-hydroxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 19013-10-6
ethyl 4-hydroxy-3-nitrobenzoate

: 886983-43-3
ethyl 3-{2-[(triphenylmethylsulfanyl)methylcarbonylamino]ethanamido}-4-hydroxybenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / H₂ / Pd/C / methanol / 2 h / 760 Torr

2: 92 percent / 4-(dimethylamino)pyridine / acetonitrile / 3 h / 60 °C

With dmap; hydrogen; palladium on activated charcoal; In methanol; acetonitrile;
DOI:10.1016/j.bmc.2005.12.005

Reference yield:

: 616-82-0
3-nitro-4-hydroxybenzoic acid

: 886983-43-3
ethyl 3-{2-[(triphenylmethylsulfanyl)methylcarbonylamino]ethanamido}-4-hydroxybenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / HCl / 20 °C

2: 92 percent / H₂ / Pd/C / methanol / 2 h / 760 Torr

3: 92 percent / 4-(dimethylamino)pyridine / acetonitrile / 3 h / 60 °C

With hydrogenchloride; dmap; hydrogen; palladium on activated charcoal; In methanol; acetonitrile;
DOI:10.1016/j.bmc.2005.12.005

Reference yield:

: 1571-72-8
3-amino-4-hydroxybenzoic acid

: 886983-43-3
ethyl 3-{2-[(triphenylmethylsulfanyl)methylcarbonylamino]ethanamido}-4-hydroxybenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 40 percent / HCl

2: 92 percent / 4-(dimethylamino)pyridine / acetonitrile / 3 h / 60 °C

With hydrogenchloride; dmap; In acetonitrile;
DOI:10.1016/j.bmc.2005.12.005