methyl 3-amino-3-N-benzoyl-3-deoxy-2,3-(internal carbamate)-4,6-O-(phenylmethylene)-β-D-allopyranoside

Base Information

Chemical Name:methyl 3-amino-3-N-benzoyl-3-deoxy-2,3-(internal carbamate)-4,6-O-(phenylmethylene)-β-D-allopyranoside
CAS No.:129263-22-5
Molecular Formula:C₂₂H₂₁NO₇
Molecular Weight:411.411
Hs Code.:

Synonyms:methyl 3-amino-3-N-benzoyl-3-deoxy-2,3-(internal carbamate)-4,6-O-(phenylmethylene)-β-D-allopyranoside

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Chemical Property of methyl 3-amino-3-N-benzoyl-3-deoxy-2,3-(internal carbamate)-4,6-O-(phenylmethylene)-β-D-allopyranoside

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Technology Process of methyl 3-amino-3-N-benzoyl-3-deoxy-2,3-(internal carbamate)-4,6-O-(phenylmethylene)-β-D-allopyranoside

There total 3 articles about methyl 3-amino-3-N-benzoyl-3-deoxy-2,3-(internal carbamate)-4,6-O-(phenylmethylene)-β-D-allopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 129217-39-6
methyl 2-O-(benzoylcarbamyl)-4,6-O-(phenylmethylene)-3-O-<(trifluoromethyl)sulfonyl>-β-D-glucopyranoside

: 129263-23-6
(3aR,4R,5aR,8R,9aS,9bR)-4-Methoxy-8-phenyl-hexahydro-3,5,7,9-tetraoxa-1-aza-cyclopenta[a]naphthalen-2-one

: 129263-22-5
methyl 3-amino-3-N-benzoyl-3-deoxy-2,3-(internal carbamate)-4,6-O-(phenylmethylene)-β-D-allopyranoside

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 0 ℃; for 3h;
DOI:10.1021/jo00309a013

Reference yield:

: 129217-31-8
methyl 4,6-O-(phenylmethylene)-3-O-<(trifluoromethyl)sulfonyl>-β-D-glucopyranoside

: 129263-22-5
methyl 3-amino-3-N-benzoyl-3-deoxy-2,3-(internal carbamate)-4,6-O-(phenylmethylene)-β-D-allopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: CCl₄ / 25 °C

2: 37 percent / NaH / tetrahydrofuran / 3 h / 0 °C

With sodium hydride; In tetrahydrofuran; tetrachloromethane;
DOI:10.1021/jo00309a013

Reference yield:

: 4461-33-0
benzoyl isocyanate

: 129263-22-5
methyl 3-amino-3-N-benzoyl-3-deoxy-2,3-(internal carbamate)-4,6-O-(phenylmethylene)-β-D-allopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: CCl₄ / 25 °C

2: 37 percent / NaH / tetrahydrofuran / 3 h / 0 °C

With sodium hydride; In tetrahydrofuran; tetrachloromethane;
DOI:10.1021/jo00309a013