chlorobis[[(diphenylphosphino)ethyl]dimethylsilyl]iridium(III)

Base Information

• Chemical Name: chlorobis[[(diphenylphosphino)ethyl]dimethylsilyl]iridium(III)
• CAS No.: 93842-30-9
• Molecular Formula: C₃₂H₄₀ClIrP₂Si₂
• Molecular Weight: 770.461

Synonyms:chlorobis[[(diphenylphosphino)ethyl]dimethylsilyl]iridium(III)

Chemical Property of chlorobis[[(diphenylphosphino)ethyl]dimethylsilyl]iridium(III)

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

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Technology Process of chlorobis[[(diphenylphosphino)ethyl]dimethylsilyl]iridium(III)

There total 1 articles about chlorobis[[(diphenylphosphino)ethyl]dimethylsilyl]iridium(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

chloro(1,5-cyclooctadiene)iridium(I) dimer + 2-dimethylsilyl-1-diphenylphosphinoethane (86934-58-9) → chlorobis[[(diphenylphosphino)ethyl]dimethylsilyl]iridium(III) (93842-30-9)

Guidance literature:

In tetrahydrofuran; reagents were mixed and stirred for 30 min; Et2O was added; elem.anal.;

Reference yield: 95.0%

chlorobis[[(diphenylphosphino)ethyl]dimethylsilyl]iridium(III) (93842-30-9) + tert-butylisonitrile (119072-55-8,7188-38-7) → [Ir((C6H5)2PCH2CH2Si(CH3)2)2(Cl)(CNC(CH3)3)] (93842-45-6)

Guidance literature:

In tetrahydrofuran; reagents were mixed; solvent was removed, Et2O was added; elem.anal.;

Reference yield: 81.0%

chlorobis[[(diphenylphosphino)ethyl]dimethylsilyl]iridium(III) (93842-30-9) + trifluorophosphane (7783-55-3) → [Ir((C6H5)2PCH2CH2Si(CH3)2)2(Cl)(PF3)] (93842-42-3)

Guidance literature:

In tetrahydrofuran; PF3 was bubbled through a soln. of complex; solvent was removed, hexane was added; elem.anal.;

upstream raw materials:

2-dimethylsilyl-1-diphenylphosphinoethane

Downstream raw materials:

Ir(P(C₆H₅)2CH₂CH₂Si(CH₃)2)2(H)(CO)

iodobis[[(diphenylphosphino)ethyl]dimethylsilyl]iridium(III)

bromobis[[(diphenylphosphino)ethyl]dimethylsilyl]iridium(III)

[Ir((C₆H₅)2PCH₂CH₂Si(CH₃)2)2(Cl)(PF₃)]

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